Six-axis multi-anvil press for high-pressure, high-temperature neutron diffraction experiments

被引:44
|
作者
Sano-Furukawa, A. [1 ,2 ]
Hattori, T. [1 ,2 ]
Arima, H. [3 ]
Yamada, A. [4 ]
Tabata, S. [5 ]
Kondo, M. [5 ]
Nakamura, A. [5 ]
Kagi, H. [6 ]
Yagi, T. [6 ]
机构
[1] Japan Atom Energy Agcy, Quantum Beam Sci Ctr, Ibaraki 3191195, Japan
[2] Japan Atom Energy Agcy, J PARC Ctr, Ibaraki 3191195, Japan
[3] Tohoku Univ, Inst Mat Res, Sendai, Miyagi 9808577, Japan
[4] Univ Shiga Prefecture, Hikone, Shiga 5228533, Japan
[5] Sumitomo Heavy Ind Co Ltd, Saijo, Ehime 7920001, Japan
[6] Univ Tokyo, Grad Sch Sci, Geochem Res Ctr, Tokyo 1130033, Japan
来源
REVIEW OF SCIENTIFIC INSTRUMENTS | 2014年 / 85卷 / 11期
关键词
POWDER DIFFRACTION; APPARATUS; CELL;
D O I
10.1063/1.4901095
中图分类号
TH7 [仪器、仪表];
学科分类号
0804 ; 080401 ; 081102 ;
摘要
We developed a six-axis multi-anvil press, ATSUHIME, for high-pressure and high-temperature in situ time-of-flight neutron powder diffraction experiments. The press has six orthogonally oriented hydraulic rams that operate individually to compress a cubic sample assembly. Experiments indicate that the press can generate pressures up to 9.3 GPa and temperatures up to 2000 K using a 6-6-type cell assembly, with available sample volume of about 50 mm(3). Using a 6-8-type cell assembly, the available conditions expand to 16 GPa and 1273 K. Because the six-axis press has no guide blocks, there is sufficient space around the sample to use the aperture for diffraction and place an incident slit, radial collimators, and a neutron imaging camera close to the sample. Combination of the six-axis press and the collimation devices realized high-quality diffraction pattern with no contamination from the heater or the sample container surrounding the sample. This press constitutes a new tool for using neutron diffraction to study the structures of crystals and liquids under high pressures and temperatures. (C) 2014 AIP Publishing LLC.
引用
收藏
页数:8
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