One-pot synthesis of benzylacetamide from oxime under ultrasound irradiation

被引:10
|
作者
Li, Ji-Tai [1 ]
Meng, Xian-Tao [1 ]
Zhai, Xin-Li [1 ]
机构
[1] Hebei Univ, Coll Chem & Environm Sci, Key Lab Analyt Sci & Technol Hebei Prov, Baoding 071002, Peoples R China
关键词
Benzylacetamide; Preparation; One-pot reaction; Ultrasound irradiation; Reduction and acetylation; AMMONIUM FORMATE; AMINES; REDUCTION; TRANSAMIDATION; ACETYLATION; CATALYST; CHLORIDE; SYSTEM;
D O I
10.1016/j.ultsonch.2008.11.007
中图分类号
O42 [声学];
学科分类号
070206 ; 082403 ;
摘要
One-pot synthesis of benzylacetamide from oxime can be carried out in 80-95% yield at 35-40 degrees C under ultrasound irradiation. This method provided several advantages such as simple work-up procedure, shorter reaction time and higher yield. (C) 2008 Elsevier B.V. All rights reserved.
引用
收藏
页码:590 / 592
页数:3
相关论文
共 50 条
  • [21] A convenient one-pot synthesis of dibenzyl diselenides under microwave irradiation conditions
    Wang, JX
    Lin, B
    Li, WB
    Hu, YL
    SYNTHETIC COMMUNICATIONS, 2000, 30 (02) : 325 - 332
  • [22] One-pot synthesis of sulfonamides from methyl sulfinates using ultrasound
    Garcia Ruano, Jose L.
    Parra, Alejandro
    Marzo, Leyre
    Yuste, Francisco
    Mastranzo, Virginia M.
    TETRAHEDRON, 2011, 67 (16) : 2905 - 2910
  • [23] Facile one-pot green synthesis of tetrahydrobiphenylene-1,3-dicarbonitriles in aqueous media under ultrasound irradiation
    Nhlanhla Gracious Shabalala
    Suresh Maddila
    Sreekantha B. Jonnalagadda
    Research on Chemical Intermediates, 2016, 42 : 8097 - 8108
  • [24] A one-pot three-component synthesis of novel α-sulfamidophosphonates under ultrasound irradiation and catalyst-free conditions
    Belhani, Billel
    Berredjem, Malika
    Le Borgne, Marc
    Bouaziz, Zouhair
    Lebreton, Jacques
    Aouf, Nour-Eddine
    RSC ADVANCES, 2015, 5 (49) : 39324 - 39329
  • [25] Facile one-pot green synthesis of tetrahydrobiphenylene-1,3-dicarbonitriles in aqueous media under ultrasound irradiation
    Shabalala, Nhlanhla Gracious
    Maddila, Suresh
    Jonnalagadda, Sreekantha B.
    RESEARCH ON CHEMICAL INTERMEDIATES, 2016, 42 (12) : 8097 - 8108
  • [26] Rapid One-Pot Synthesis of Alkane-α,ω-Diylbisphosphonic Acids from Dihalogenoalkanes Under Microwave Irradiation
    Villemin, Didier
    Moreau, Bernard
    Kaid, M'hamed
    Didi, Mohamed Amine
    PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS, 2010, 185 (08) : 1583 - 1586
  • [27] An efficient one-pot synthesis of nitriles from carboxylic acids without solvent under microwave irradiation
    Feng, JC
    Liu, B
    Liu, Y
    Li, CC
    SYNTHETIC COMMUNICATIONS, 1996, 26 (24) : 4545 - 4548
  • [28] An efficient one-pot synthesis of nitriles from carboxylic acids without solvent under microwave irradiation
    Department of Chemistry, Nanjing University, Nanjing 210093, China
    不详
    SYNTH. COMMUN., 24 (4545-4548):
  • [29] One-pot easy conversion of Baylis-Hillman adducts into arylpyrazoles under ultrasound irradiation
    Mamaghani, Manouchehr
    Dastmard, Sahar
    ARKIVOC, 2009, : 168 - 173
  • [30] An efficient and solvent-free one-pot synthesis of dihydropyrimidinones under microwave irradiation
    Jiang, Cheng
    You, Qi Dong
    CHINESE CHEMICAL LETTERS, 2007, 18 (06) : 647 - 650