Simultaneous capillary GC-MS determination of triazines and amides in water

被引：11
|
作者：
Hu, R
Berthion, JM
Bodereau, I
Fournier, J
机构：
[1] LAB DEPT SARTHE,F-72004 LE MANS,FRANCE
[2] CTR REG ETUD PROD AGROPHARMACEUT,F-49070 BEAUCOUZE,FRANCE
[3] SICHUAN ACAD AGR SCI,CENT LAB,CHENGDU,SICHUAN,PEOPLES R CHINA
来源：
CHROMATOGRAPHIA | 1996年 / 43卷 / 3-4期
关键词：
gas chromatography mass spectrometry; triazines; amides; water pollution;
D O I：
10.1007/BF02292948
中图分类号：
Q5 [生物化学];
学科分类号：
071010 ; 081704 ;
摘要：
A simultaneous capillary Gas Chromatographic-Mass Spectrometric (GC-MS) method is described for the determination of thirteen pesticides belonging to the triazine and amide families in water. The sample is extracted in liquid-liquid mode (dichloromethane) and then the determination of the residues is carried out by capillary gas chromatography with mass spectrometric detection in the Selected-Ion Monitoring mode (SIM). The average recoveries of spiked compounds are in the 78.4-135.4 % range between the relative low level (0.100 mu g L(-1)) and the relative high level (10.0 mu g L(-1)). The limits of detection (LOD) are in the 0.009-0.128 mu g L(-1) range.
引用
收藏
页码：181 / 186
页数：6
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