Hydrothermal synthesis and crystal structure of a novel 4,4′-bipyridine bridging dumbbell-like dimeric pentamolybdate:: [4,4′-H2bipy]3[4,4′-Hbipy]2[(Mo5O17)2(4,4′-bipy)]

被引：9

作者：

Niu, JY ^{[1
]}

Wang, ZL ^{[1
]}

Wang, JP ^{[1
]}

机构：

[1] Henan Univ, Sch Chem & Chem Engn, Kaifeng 475001, Peoples R China

来源：

INORGANIC CHEMISTRY COMMUNICATIONS | 2004年 / 7卷 / 04期

关键词：

polyoxometalates; hydrothermal synthesis; crystal structure; molybdenum;

D O I：

10.1016/j.inoche.2004.02.018

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

A novel dimeric pentamolybdate [4,4'-H(2)bipy](3)[4,4'-Hbipy](2)[(Mo5O17)(2)(4,4'-bipy)], the first example of a 4,4'-bipyridine bridging dumbbell-like polyoxomolybdates, has been prepared by hydrothermal synthesis and characterized by X-ray crystallography. (C) 2004 Elsevier B.V. All rights reserved.

引用

页码：556 / 558

页数：3

共 50 条

[41] Rectangular grid two-dimensional sheets of copper(II) bridged by both co-ordinated and hydrogen bonded 4,4'-bipyridine (4,4'-bipy) in [Cu(mu-4,4'-bipy)(H2O)(2)(FBF3)(2)]center dot 4,4'-bipy
Blake, AJ
Hill, SJ
Hubberstey, P
Li, WS
JOURNAL OF THE CHEMICAL SOCIETY-DALTON TRANSACTIONS, 1997, (06): : 913 - 914
[42] In Situ Preparation, Crystal Structure and Fluorescence of [(CH3)2-4,4′-H2bipy][FeCl4]2 (Bipy = Bipyridine)
Chen, Wen-Tong
Chen, Hua-Long
Kuang, Han-Mao
SYNTHESIS AND REACTIVITY IN INORGANIC METAL-ORGANIC AND NANO-METAL CHEMISTRY, 2014, 44 (01) : 130 - 132
[43] Synthesis, characterization and crystal structure of an inorganic-organic composite metatungstate:: [Co(4,4′-bipy)2(H2O)4](4,4′-H2bipy)2[H2W12O40]•5.5H2O
Zhou Da-Peng
Ren Qing
Zhao Jun-Wei
Wang Jing-Ping
CHINESE JOURNAL OF STRUCTURAL CHEMISTRY, 2007, 26 (11) : 1287 - 1292
[44] Synthesis,Characterization and Crystal Structure of an Inorganic-organic Composite Metatungstate:[Co（4,4′-bipy）2（H2O）4]（4,4′-H2bipy）2[H2W12O40]·5.5H2O
周大鹏
任请
赵俊伟
王敬平
Chinese Journal of Structural Chemistry, 2007, (11) : 1287 - 1292
[45] Infinite chain structures of [Zn(4,4′-bipy)Cl2]n and [Cu(H2PO4)(4,4′-bipy)•2H2O]n via hydrothermal synthesis
Liang, YC
Hong, MC
Cao, R
Su, WP
Zhao, YJ
Weng, JB
POLYHEDRON, 2001, 20 (19) : 2477 - 2481
[46] Two new Pb(II) coordination polymers, [Pb2(μ-4,4'-bipy) (μ-2-sb)2(DMF)]n and {[Pb2(μ-4,4'-bipy) (μ-2-sb)2(H2O)2] • H2O}n (4,4'-bipy=4,4'-bipyridine and 2-H2sb=2-sufobenzoic acid)
Xiao, Hong-Ping
Wang, Jia-Guo
Morsali, Ali
Zhang, Wei-Bing
Li, Xin-Hua
JOURNAL OF COORDINATION CHEMISTRY, 2008, 61 (22) : 3703 - 3710
[47] Structure of coordination polymer, [Zn(bipy)(H2O)3SO4] • 2H2O (bipy=4,4′-bipyridine)
Ma, JF
Liu, JF
Xing, Y
Jia, HQ
Lin, YH
CHINESE JOURNAL OF STRUCTURAL CHEMISTRY, 2000, 19 (02) : 103 - 106
[48] Synthesis, structure and properties of a 4,4′-bipyridine bridged dinuclear Cu(II) complex:: {Cu2(4,4′-bipy)[HOCH2CH2N(CH2CH2NH2)2]2}•(ClO4)4 • 1/2(4,4′-bipy)•4H2O
Gao, J
Xu, XY
Wang, MY
Liu, QL
Song, HB
JOURNAL OF COORDINATION CHEMISTRY, 2005, 58 (15) : 1351 - 1360
[49] Structure of Coordination Polymer, 〔Zn(bipy)(H2O)3SO4〕·2H2O (bipy=4,4'-bipyridine)
MA Jian Fang a LIU Jing Fu a XING Yan b JIA Heng Qing b LIN Yong Hua b a (Department of Chemistry
结构化学, 2000, (02) : 103 - 106
[50] SYNTHESIS, CHARACTERIZATION AND MAGNETIC-PROPERTIES OF ONE-DIMENSIONAL 4,4'-BIPYRIDINE-BRIDGED MANGANESE(II) COMPLEX - CRYSTAL-STRUCTURE OF [MN(MU-4,4'-BIPY)(4,4'-BIPY)(NCS)(2)(H2O)(2)](N)
LI, MX
XIE, GY
GU, YD
CHEN, J
ZHENG, PJ
POLYHEDRON, 1995, 14 (09) : 1235 - 1239

← 1 2 3 4 5 →