Citrus limetta juice as capping agent in hydrothermal synthesis of ZnS nanosphere for photocatalytic activity

被引:41
|
作者
Samanta, Dhrubajyoti [1 ]
Chanu, T. Inakhunbi [1 ]
Chatterjee, Somenath [1 ,2 ]
机构
[1] Sikkim Manipal Univ, Ctr Mat Sci & Nanotechnol, Sikkim Manipal Inst Technol, Sikkim, India
[2] Sikkim Manipal Univ, Sikkim Manipal Inst Technol, Elect & Commun Engn Dept, Sikkim, India
关键词
Chemical synthesis; Sol-gel chemistry; X-ray diffraction; Transmission electron microscopy (TEM); Catalytic properties; ASSISTED SYNTHESIS; SILVER NANOPARTICLES; NANOSTRUCTURES; DEGRADATION; FABRICATION; EMISSION; FRUITS;
D O I
10.1016/j.materresbull.2016.11.019
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
ZnS nanospheres have been synthesized by a simple cost-effective hydrothermal method using Citrus limetta juice as a capping agent. The morphology and composition of the synthesized material have been characterized by X-ray diffraction (XRD), Fourier transform infra-red spectroscopy (FUR), energy dispersed X-ray spectrometry (EDS), field emission scanning electron microscopy (FESEM), high resolution transmission electron microscopy (HRTEM), ultraviolet-visible (UV-VIS) spectroscopy and room temperature photoluminescence spectroscopy (PL). HRTEM images confirm that the particles are nanospheres. Multiple defect emission of the ZnS nanospheres was noticed from PL study. The photocatalytic experiment indicates the potential degradation (83%) of Rhodamine B (RhB) under solar radiation due to the presence of the synthesized Zns nanospheres. (C) 2016 Elsevier Ltd. All rights reserved.
引用
收藏
页码:85 / 90
页数:6
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