Properties of BaTiO3 synthesized from barium titanyl oxalate

被引:22
|
作者
Kim, Jong-Hyun [1 ]
Jung, Won-Sik [1 ]
Kim, Hyun-Tae [1 ]
Yoon, Dang-Hyok [1 ]
机构
[1] Yeungnam Univ, Sch Mat Sci & Engn, Kyongsan 712749, South Korea
关键词
Firing; Dielectric properties; BaTiO3 and titanates; Capacitors; PARTICLE-SIZE; POWDER; TETRAGONALITY; DEPENDENCE; TRANSITION;
D O I
10.1016/j.ceramint.2009.01.006
中图分类号
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
In order to enhance the tetragonality of BaTiO3 derived from barium titanyl oxalate (BTO), various treatments were carried out by considering the thermal decomposition mechanism of BTO in air. A multi-step heat treatment process and the addition of carbon black, as a particle growth inhibitor, were effective in increasing the tetragonality, whilst maintaining a particle size smaller than 200 nm. The synthesized BaTiO3 powder with a mean particle size of 177 urn showed a tetragonality and K-factor of 1.0064 and approximately 3, respectively. (C) 2009 Elsevier Ltd and Techna Group S.r.l. All rights reserved.
引用
收藏
页码:2337 / 2342
页数:6
相关论文
共 50 条
  • [21] Preparation of highly dispersed barium titanate nanoparticles from barium titanyl oxalate nanoparticles and their dielectric properties
    Wada, Satoshi
    Kondo, Shuhei
    Moriyoshi, Chikako
    Kuroiwa, Yoshihiro
    Japanese Journal of Applied Physics, 2008, 47 (9 PART 2): : 7612 - 7616
  • [22] REEXAMINATION OF BARIUM TITANYL OXALATE TETRAHYDRATE
    FANG, TT
    LIN, HB
    HWANG, JB
    JOURNAL OF MATERIALS SCIENCE LETTERS, 1990, 9 (06) : 688 - 690
  • [23] Synthesis of barium titanyl oxalate by homogeneous precipitation from dimethyl oxalate solution
    Lim, M
    Huh, W
    Lee, C
    BULLETIN OF THE KOREAN CHEMICAL SOCIETY, 1998, 19 (06) : 702 - 706
  • [24] Particle size control of barium titanate prepared from barium titanyl oxalate
    Park, ZH
    Shin, HS
    Lee, BK
    Cho, SH
    JOURNAL OF THE AMERICAN CERAMIC SOCIETY, 1997, 80 (06) : 1599 - 1604
  • [25] Properties of barium titanate powders in relation to the heat treatment of the barium titanyl oxalate precursor
    Shut, V. N.
    Kostomarov, S. V.
    INORGANIC MATERIALS, 2012, 48 (06) : 613 - 618
  • [26] Particle size control of barium titanate prepared from barium titanyl oxalate
    Park, Zee Hoon
    Shin, Hyo Soon
    Lee, Byung Kyo
    Cho, Sang Hee
    1997, American Ceramic Soc, Westerville, OH, United States (80)
  • [27] Properties of barium titanate powders in relation to the heat treatment of the barium titanyl oxalate precursor
    V. N. Shut
    S. V. Kostomarov
    Inorganic Materials, 2012, 48 : 613 - 618
  • [28] Dielectric properties of sintered BaTiO3 prepared from barium acetate and titanium dioxide
    Othman, Kolthoum, I
    Ali, M. El Sayed
    El-Hout, S.
    KUWAIT JOURNAL OF SCIENCE, 2019, 46 (03) : 53 - 59
  • [29] Dielectric properties of BaTiO3 synthesized by containerless processing technique
    Yu, JD
    Paradis, PF
    Ishikawa, T
    Yoda, S
    JOURNAL OF THE KOREAN PHYSICAL SOCIETY, 2005, 46 (01) : 15 - 18
  • [30] Electrorheological properties of polyaniline-modidied barium titanyl oxalate particles
    Liu, Yang-Sheng
    Guan, Jian-Guo
    Ma, Hui-Ru
    Gongneng Cailiao/Journal of Functional Materials, 2008, 39 (11): : 1832 - 1834