In Situ Observation of Oxidation of Liquid Droplets of Tin and Melting Behavior of a Tin Particle Covered With a Tin Oxide Layer

被引：3
|
作者：
Mima, Takayuki [2 ]
Takeuchi, Hironori [2 ]
Arai, Shigeo [1 ]
Kishita, Keisuke [3 ]
Kuroda, Kotaro [2 ]
Saka, Hiroyasu [1 ]
机构：
[1] Nagoya Univ, Ecotopia Sci Inst, 1MV Electron Microscopy Lab, Nagoya, Aichi 4648603, Japan
[2] Nagoya Univ, Grad Sch Engn, Nagoya, Aichi 4648603, Japan
[3] Toyota Motor Co Ltd, Mat Anal Dept, Toyota 4718542, Japan
来源：
MICROSCOPY RESEARCH AND TECHNIQUE | 2009年 / 72卷 / 03期
关键词：
liquid metal; solid-liquid interface; oxidation; TRANSMISSION ELECTRON-MICROSCOPY; GROWTH-PROCESS; INSITU OBSERVATION; INTERFACE; CRYSTAL; BI;
D O I：
10.1002/jemt.20675
中图分类号：
R602 [外科病理学、解剖学]; R32 [人体形态学];
学科分类号：
100101 ;
摘要：
Oxidation of a liquid droplet of tin (Sn) was observed using an in situ specimen heating holder in an oxygen environment. The surface of the Sn liquid droplet was covered with a tin oxide layer, Sn3O4, the thickness of which depended on the oxygen pressure and temperature. Subsequent cooling of the droplet resulted in the formation of a solid Sn particle covered with a Sn3O4 layer. The solid Sn particle was then heated above the melting temperature of Sn, and the melting behavior of Sn was observed. Microsc. Res. Tech. 72:223-231, 2009. (C) 2009 Wiley-Liss, Inc.
引用
收藏
页码：223 / 231
页数：9
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