In Situ Observation of Oxidation of Liquid Droplets of Tin and Melting Behavior of a Tin Particle Covered With a Tin Oxide Layer

被引：3

作者：

Mima, Takayuki ^{[2
]}

Takeuchi, Hironori ^{[2
]}

Arai, Shigeo ^{[1
]}

Kishita, Keisuke ^{[3
]}

Kuroda, Kotaro ^{[2
]}

Saka, Hiroyasu ^{[1
]}

机构：

[1] Nagoya Univ, Ecotopia Sci Inst, 1MV Electron Microscopy Lab, Nagoya, Aichi 4648603, Japan

[2] Nagoya Univ, Grad Sch Engn, Nagoya, Aichi 4648603, Japan

[3] Toyota Motor Co Ltd, Mat Anal Dept, Toyota 4718542, Japan

来源：

MICROSCOPY RESEARCH AND TECHNIQUE | 2009年 / 72卷 / 03期

关键词：

liquid metal; solid-liquid interface; oxidation; TRANSMISSION ELECTRON-MICROSCOPY; GROWTH-PROCESS; INSITU OBSERVATION; INTERFACE; CRYSTAL; BI;

D O I：

10.1002/jemt.20675

中图分类号：

R602 [外科病理学、解剖学]; R32 [人体形态学];

学科分类号：

100101 ;

摘要：

Oxidation of a liquid droplet of tin (Sn) was observed using an in situ specimen heating holder in an oxygen environment. The surface of the Sn liquid droplet was covered with a tin oxide layer, Sn3O4, the thickness of which depended on the oxygen pressure and temperature. Subsequent cooling of the droplet resulted in the formation of a solid Sn particle covered with a Sn3O4 layer. The solid Sn particle was then heated above the melting temperature of Sn, and the melting behavior of Sn was observed. Microsc. Res. Tech. 72:223-231, 2009. (C) 2009 Wiley-Liss, Inc.

引用

页码：223 / 231

页数：9

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