(1R,2S)-benzyl N-[3-(diisopropylaminocarbonyl)-2-phenylprop-3-enyl]carbamate

被引:0
|
作者
Qu, Hongchang [1 ]
Carducci, Michael D. [1 ]
Nichol, Gary S. [1 ]
Hruby, Victor J. [1 ]
机构
[1] Univ Arizona, Dept Chem, Tucson, AZ 85721 USA
来源
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2006年 / 62卷
关键词
D O I
10.1107/S1600536806032041
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
The title compound, C25H32N2O3, was synthesized as part of a series of related compounds using a modified Eschenmoser-Claisen rearrangement reaction. The compound is racemic and the structure features a centrosymmetric hydrogen-bonded dimerization along with some aromatic stacking stabilization.
引用
收藏
页码:O3921 / O3922
页数:2
相关论文
共 50 条
  • [11] (1R,2S,5R)-2-Isopropyl-5-methylcyclohexyl (2S,3S)-3-phenyloxirane-2-carboxylate
    Jian, SZ
    Wang, YG
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2005, 61 : O1135 - O1136
  • [12] (1R*,2S*,3R*,4S*)-N-(1-Naphthyl)-5-norbornene-2,3-dicarboximide
    Tian, De-Mei
    Xiong, Chuan-Xi
    Dong, Li-Jie
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2007, 63 : O2393 - O2394
  • [13] Synthesis of (1R,2S)- and (1S,2S)-3-azido-1,2-dihydroxypropylphosphonates
    Wróblewski, AE
    Glowacka, IE
    TETRAHEDRON-ASYMMETRY, 2002, 13 (09) : 989 - 994
  • [14] (+)-(1R,2S,3R)-2-[(Benzyloxycarbonyl)methyl]-3-phenylcyclopropanecarboxylic acid
    Avery, Thomas D.
    Greatrex, Ben W.
    Taylor, Dennis K.
    Tiekink, Edward R. T.
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2007, 63 : O3344 - U4683
  • [15] (1R,2S)-2-[(S)-(P-CHLOROPHENYL)SULFINYL]-N,N,3,3-TETRAMETHYLCYCLOPROPYLAMINE
    CHIDESTER, CG
    DUCHAMP, DJ
    ACTA CRYSTALLOGRAPHICA SECTION B-STRUCTURAL SCIENCE, 1977, 33 (JAN15): : 221 - 223
  • [16] Benzyl 3-[(E,E)-3-phenylprop-2-enylidene]dithiocarbazate
    Tarafder, M. T. H.
    Crouse, K. A.
    Islam, M. Toihidul
    Chantrapromma, Suchada
    Fun, Hoong-Kun
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2008, 64 : O1042 - U1871
  • [17] Synthesis of a New Chiral Carbamate: 2-nitrophenyl(1R,2S)-(1,2-diphenyl-2-hydroxyethyl)carbamate
    Kecseti, Ildiko Mariana
    Simon, Monika
    Csunderlik, Carol
    REVISTA DE CHIMIE, 2010, 61 (08): : 759 - 761
  • [18] Synthesis of (2R,3S)-((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl) 2-(4-bromophenyl)-3-(tert-butoxy-carbonylamino)-tetrahydrofuran-3-carboxylate and (2S,3R)-((1R,2S,5R)-2-isopropyl-5-methylcyclohexyl) 2-(4-bromophenyl)-3-(tert-butoxycarbonylamino)-tetrahydrofuran-3-carboxylate
    Grauer, Andreas
    Koenig, Burkhard
    MOLBANK, 2009, (01)
  • [19] tert-Butyl N-[(1R,2R)-2-(isothiocyanato)-cyclohexyl]carbamate
    Zhong, Ming
    Siegler, Maxime
    Long, Sihui
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2007, 63 : O3589 - U4253
  • [20] Synthesis of (1R,2S)- and (1S,2S)-3-(4-carbamoyl-1,2,3-triazol-1-yl)-1,2-dihydroxypropylphosphonates
    Wróblewski, AE
    Glowacka, IE
    TETRAHEDRON-ASYMMETRY, 2004, 15 (09) : 1457 - 1464