Synthesis, crystal structure and study of X-H•••A interactions in N,N′-bis-(4-methoxy-benzylidine)-hydrazine

被引：0
|
作者：
Rajnikant [1 ]
Dinesh
Deshmukh, M. B.
Kamni
机构：
[1] Univ Jammu, Postgrad Dept Phys, Condensed Matter Phys Grp, Jammu 180006, India
[2] Shivaji Univ, Dept Chem, Kolhapur 416004, Maharashtra, India
来源：
INDIAN JOURNAL OF PURE & APPLIED PHYSICS | 2006年 / 44卷 / 08期
关键词：
crystal structure; hydrazines; intra- and intermolecular interactions; alkaloid;
D O I：
暂无
中图分类号：
O4 [物理学];
学科分类号：
0702 ;
摘要：
Synthesis and crystal structure of N,N'-bis-(4-methoxy-benzylidine)-hydrazine have been reported in this paper. The title compound crystallizes in the monoclinic space group C2/c with unit cell parameters a = 17.416(3), b = 10.711(3) and c =8.428(3)angstrom, beta =113.64(2)degrees, V = 1440.2(8)angstrom(3) and Z = 4. The structure has been refined to a R-value of 0.038 for 937 observed reflections. The molecules adopt columnar packing in the unit cell and the crystal structure is stabilized by two intra- and five intermolecular hydrogen bonded interactions.
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页码：602 / 605
页数：4
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