Synthesis, crystal structure and study of X-H•••A interactions in N,N′-bis-(4-methoxy-benzylidine)-hydrazine

被引：0
|
作者：
Rajnikant [1 ]
Dinesh
Deshmukh, M. B.
Kamni
机构：
[1] Univ Jammu, Postgrad Dept Phys, Condensed Matter Phys Grp, Jammu 180006, India
[2] Shivaji Univ, Dept Chem, Kolhapur 416004, Maharashtra, India
来源：
INDIAN JOURNAL OF PURE & APPLIED PHYSICS | 2006年 / 44卷 / 08期
关键词：
crystal structure; hydrazines; intra- and intermolecular interactions; alkaloid;
D O I：
暂无
中图分类号：
O4 [物理学];
学科分类号：
0702 ;
摘要：
Synthesis and crystal structure of N,N'-bis-(4-methoxy-benzylidine)-hydrazine have been reported in this paper. The title compound crystallizes in the monoclinic space group C2/c with unit cell parameters a = 17.416(3), b = 10.711(3) and c =8.428(3)angstrom, beta =113.64(2)degrees, V = 1440.2(8)angstrom(3) and Z = 4. The structure has been refined to a R-value of 0.038 for 937 observed reflections. The molecules adopt columnar packing in the unit cell and the crystal structure is stabilized by two intra- and five intermolecular hydrogen bonded interactions.
引用
收藏
页码：602 / 605
页数：4
相关论文
共 50 条
  • [1] Crystal structure of N,N-bis(4-hydroxy-benzylidine)ethylenediamine•methanol
    Hökelek, T
    Ünaleroglu, C
    ANALYTICAL SCIENCES, 2001, 17 (05) : 679 - 680
  • [2] Crystal structure of N,N′-bis(4-methoxy-benzylidene)hydrazine, C16H16N2O2
    Jin, Jian-Yu
    Zhang, Kang
    Zhang, Li-Xue
    Zhang, An-Jiang
    Liu, Yu-Zhen
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2007, 222 (04): : 391 - 392
  • [3] Crystal Structure of N,N-Bis(4-hydroxy-benzylidine)ethylenediamine•methanol
    Tuncer Hökelek
    Canan Ünaleroğlu
    Analytical Sciences, 2001, 17 : 679 - 680
  • [4] Synthesis, Crystal Structure and DNA Binding Studies of Bis(piperidinium) bis-(N,N,N′,N′-tetramethylethylenediammonium) Decavanadate(V) Tetrahydrate
    Jiang, M.
    Han, Y. -T.
    Li, Y. -T.
    Wu, Z. -Y.
    Yan, C. -W.
    POLISH JOURNAL OF CHEMISTRY, 2009, 83 (11) : 1849 - 1858
  • [5] CRYSTAL AND MOLECULAR-STRUCTURE OF N,N,N',N'-BIS-(HEXAMETHYLENE)THIURAMDISULFIDE
    POLYAKOVA, IN
    STARIKOVA, ZA
    JOURNAL OF STRUCTURAL CHEMISTRY, 1990, 31 (06) : 982 - 985
  • [6] CRYSTAL STRUCTURE OF N,N'-BIS-(4-ETHOXYPHENYL)ACETAMIDINIUM BIS-PARA-NITROPHENYLPHOSPHATE MONOHYDRATE
    SAX, M
    YOO, CS
    STEWART, JM
    ACTA CRYSTALLOGRAPHICA SECTION B-STRUCTURAL CRYSTALLOGRAPHY AND CRYSTAL CHEMISTRY, 1971, B 27 (AUG15): : 1635 - +
  • [7] CRYSTAL-STRUCTURE OF BIS-(N,N'-DIETHYLTHIOSELENOCARBAMATO)COPPER(II)
    KAISER, J
    RICHTER, R
    SIELER, J
    ACTA CRYSTALLOGRAPHICA SECTION B-STRUCTURAL SCIENCE, 1975, 31 (NOV15): : 2600 - 2603
  • [8] Crystal structure of bis-[N,N′-bis-(3-allyl salicylidene)-o-phenylene diamine]thorium (IV), C52H44N4O4Th
    He, Fang-Fang
    Wang, Hong-Qing
    Wang, Xiao-Feng
    Wang, Yu-Yuan
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2012, 227 (04): : 521 - 524
  • [9] Synthesis and crystal structure of N,N′-(p-phenyl)-bis-(p-nitro)benzoylthiourea
    Dong, Wen-Kui
    Yang, Xiao-Qing
    Chai, Lan-Qin
    Tian, Yong-Qiang
    Feng, Jian-Hua
    PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS, 2008, 183 (05) : 1181 - 1187
  • [10] SYNTHESIS AND STRUCTURE OF N,N'-BIS-(1-ADAMANTYL) FORMAMIDINE
    KREUTZBERGER, A
    SCHRODER.HH
    TETRAHEDRON LETTERS, 1971, (39) : 3635 - +
12345