Effect of Annealing Temperatures on the Morphology and Structural Properties of PVDF/MgO Nanocomposites Thin Films

被引：1
|
作者：
Rozana, M. D. [1 ]
Arshad, A. N. [1 ]
Wahid, M. H. M. [1 ]
Habibah, Z. [2 ]
Sarip, M. N. [1 ]
Rusop, M. [3 ]
机构：
[1] Univ Teknol MARA Selangor, Fac Sci Appl, Shah Alam 40450, Malaysia
[2] Univ Teknol MARA Selangor, Fac Elect Engn, Nanoelect Ctr NET, Shah Alam 40450, Malaysia
[3] Univ Teknol MARA Selangor, Inst Sci, NANO SciTech Ctr NST, Shah Alam 40450, Malaysia
来源：
8TH INTERNATIONAL CONFERENCE ON NANOSCIENCE AND NANOTECHNOLOGY 2017 (NANO-SCITECH 2017) | 2018年 / 1963卷
关键词：
BETA-PHASE TRANSFORMATION; ELECTRICAL-PROPERTIES; ALPHA;
D O I：
10.1063/1.5036881
中图分类号：
TB3 [工程材料学];
学科分类号：
0805 ; 080502 ;
摘要：
This study investigates the effect of annealing on the topography, morphology and crystal phases of poly(vinylideneflouride)/Magnesium Oxide (MgO) nanocomposites thin films via AFM, FESEM and ATR-FTIR. The nanocomposites thin films were annealed at temperatures ranging from 70 degrees C to 170 degrees C. The annealed PVDF/MgO nanocomposites thin films were then cooled at room temperature before removal from the oven. This is to restructure the crystal lattice and to reduce imperfection for the PVDF/MgO nanocomposites thin films. PVDF/MgO nanocomposites thin films with annealing temperatures of 70 degrees C, 90 degrees C and 110 degrees C showed uniform distribution of MgO nanoparticles, relatively low average surface roughness and no visible of defects. High application of annealing temperature on PVDF/MgO nanocomposites thin films caused tear-like defects on the thin films surface as observed by FESEM. The PVDF/MgO nanocomposites thin films annealed at 70 degrees C was found to be a favourable film to be utilized in this study due to its enhanced beta-crystalites of PVDF as evident in ATR-FTIR spectra.
引用
收藏
页数：6
相关论文
共 50 条
  • [21] Effect of annealing time on the structural and ferromagnetic properties of the GaMnN thin films
    Xingguo Gao
    Baoyuan Man
    Mei Liu
    Cheng Yang
    Chuansong Chen
    Applied Physics A, 2014, 114 : 1003 - 1007
  • [22] Effect of annealing on structural and optical properties of copper sulphide thin films
    Elmourabit, Fahd
    Elhassani, Abdessamad
    Lemaalem, Bouchaib
    El Moutaouakil, Amine
    Khoukh, Abdelaziz
    Narjis, Abdelfattah
    Limouny, Lhoussine
    Dlimi, Said
    MATERIALS TECHNOLOGY, 2024, 39 (01)
  • [23] Effect of annealing temperature on the structural and optical properties of ZnS thin films
    Asghar, M.
    Mahmood, K.
    Samaa, B. M.
    Rabia, S.
    Shahid, M-Y
    MATERIALS TODAY-PROCEEDINGS, 2015, 2 (10) : 5430 - 5435
  • [24] Influence of Annealing on the Structural, Morphology and Optical Properties of TiO2 Thin Films
    Abbas, Israa Akram
    Hazaa, Salah Qaddoori
    TECHNOLOGIES AND MATERIALS FOR RENEWABLE ENERGY, ENVIRONMENT AND SUSTAINABILITY (TMREES20), 2020, 2307
  • [25] Effect of Deposition Parameters and Annealing on the Morphology and Optical Properties of Pbs Thin Films
    Zaman, S.
    Asim, M. M.
    Siddique, S.
    Mahmood, S. K.
    ADVANCED MATERIALS XI, 2010, 442 : 144 - 151
  • [26] Effect of annealing on structure, morphology and optoelectronic properties of nanocrystalline CuO thin films
    Jundale, D. M.
    Pawar, S. G.
    Patil, S. L.
    Chougule, M. A.
    Godse, P. R.
    Patil, V. B.
    OPTICS: PHENOMENA, MATERIALS, DEVICES, AND CHARACTERIZATION: OPTICS 2011: INTERNATIONAL CONFERENCE ON LIGHT, 2011, 1391
  • [27] Effect of thermal annealing on morphology of pentacene thin films
    Ye, RB
    Baba, M
    Suzuki, K
    Ohishi, Y
    Mori, K
    JAPANESE JOURNAL OF APPLIED PHYSICS PART 1-REGULAR PAPERS SHORT NOTES & REVIEW PAPERS, 2003, 42 (7A): : 4473 - 4475
  • [28] Morphology and optical properties of MgO thin films on Mo(001)
    Benedetti, S.
    Benia, H. M.
    Nilius, N.
    Valeri, S.
    Freund, H. J.
    CHEMICAL PHYSICS LETTERS, 2006, 430 (4-6) : 330 - 335
  • [29] The Effect of Annealing Temperatures on Zinc Oxide Thin Films Properties for Electronic Devices Application
    Mamat, M. H.
    Sahdan, M. Z.
    Amizam, S.
    Rafaie, H. A.
    Khusaimi, Z.
    Ahmed, A. Zain
    Abdullah, S.
    Rusop, M.
    ICSE: 2008 IEEE INTERNATIONAL CONFERENCE ON SEMICONDUCTOR ELECTRONICS, PROCEEDINGS, 2008, : 566 - +
  • [30] Effect of annealing on structural properties of Co thin films and Co/Cu multilayers
    Hecker, M
    Mattern, N
    Brückner, W
    Schneider, CM
    EUROPEAN POWDER DIFFRACTION EPDIC 8, 2004, 443-4 : 193 - 196
12345