New tripodal ligand on the triphenylphosphine oxide platform with 1,2,3-triazole side arms: synthesis, structure, coordination, and extraction properties

被引：9

作者：

Kudryavtsev, Igor Y. ^{[1
]}

Bykhovskaya, Olga V. ^{[1
]}

Matveeva, Anna G. ^{[1
]}

Baulina, Tatyana V. ^{[1
]}

Pasechnik, Margarita P. ^{[1
]}

Matveev, Sergey V. ^{[1
]}

Vologzhanina, Anna V. ^{[1
]}

Turanov, Alexander N. ^{[2
]}

Karandashev, Vasilii K. ^{[3
,4
]}

Brel, Valery K. ^{[1
]}

机构：

[1] Russian Acad Sci, Nesmeyanov Inst Organoelement Cpds, Moscow, Russia

[2] Russian Acad Sci, Inst Solid State Phys, Chernogolovka, Russia

[3] Russian Acad Sci, Inst Microelect Technol Problems & High Pur Mat, Chernogolovka, Russia

[4] Natl Univ Sci & Technol MISiS, Moscow, Russia

来源：

MONATSHEFTE FUR CHEMIE | 2020年 / 151卷 / 11期

基金：

俄罗斯科学基金会;

关键词：

Click reaction; Extraction; 1,2,3-Triazole; Tripodal ligands; Palladium complex; X-ray structure determination; CARBAMOYLMETHYLPHOSPHINE OXIDE; ANION-BINDING; COMPLEXES; PALLADIUM; COPPER(II); RECEPTORS; SPECTROSCOPY; SELECTIVITY; CHEMISTRY; AFFINITY;

D O I：

10.1007/s00706-020-02702-6

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

New hybrid tripodal propeller ligands on the triphenylphosphine oxide platform with triazole rings in the side arms and alkyl and aryl substituents in the triazole fragments have been synthesized by the click reaction. Composition and structure of the prepared compounds have been established by vibrational (IR, Raman) and multinuclear (H-1,C-13,P-31) NMR spectroscopy, elemental analysis, and mass spectrometry. Coordination and extraction properties of the prepared compounds toward Pd(II) have been studied by the example of one of the ligands. Graphic abstract

引用

页码：1705 / 1713

页数：9

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