COPPER(II) IONS MEDIATED CRYSTAL FORMATION OF 3-(3-HYDROXY PHENYL)-1-PHENYL-1H-PYRAZOLE-4-CARBALDEHYDE

被引：0

作者：

Banpurkar, Anita R. ^{[1
]}

Wazalwar, Sach N. S. ^{[1
]}

Perdih, Franc ^{[2
]}

机构：

[1] Rajiv Gandhi Coll Engn Res & Technol, Dept Appl Chem, Chandrapur 442403, MS, India

[2] Univ Ljubljana, Fac Chem & Chem Technol, SI-1000 Ljubljana, Slovenia

来源：

BULLETIN OF THE CHEMICAL SOCIETY OF ETHIOPIA | 2020年 / 34卷 / 03期

关键词：

Cu2+ assisted crystal growth; Pyrazole-4-carbaldehyde; X-ray crystal study; Hydrogen bonding study; BIOLOGICAL EVALUATION; MOLECULAR DOCKING; DESIGN; DERIVATIVES; PYRAZOLE; ANTICANCER; SAR;

D O I：

10.4314/bcse.v34i3.13

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

Schiff base obtained from 3-hydroxyacetophenone and phenylhydrazine was subjected to Vilsmeier-Haack reaction to obtain 3-(3-hydroxyphenyl)-1-phenyl-1H-pyrazole-4-carbaldehyde (2). Successful formation of crystals of 2 was achieved using copper ions (Cu2+) as template. Present paper reports study of spectroscopic characterization and single-crystal X-ray study of 2. Hydrogen bonding network between 2 and water molecules enable the formation of 2D layer along ab-plane supported also by pi center dot center dot center dot pi stacking interactions of parallel molecules in head-to-head fashion.

引用

页码：589 / 596

页数：8

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