Poly[bis(phenethylammonium) [dibromidoplumbate(II)]-di-μ-bromido]]

被引：53
|
作者：
Shibuya, Kengo [1 ,2 ]
Koshimizu, Masanori [2 ,3 ]
Nishikido, Fumihiko [2 ,4 ]
Saito, Haruo [1 ,2 ]
Kishimoto, Shunji [2 ,5 ]
机构：
[1] Univ Tokyo, Grad Sch Arts & Sci, Inst Phys, Meguro Ku, Tokyo 1538902, Japan
[2] Japan Sci & Technol Agcy, CREST, Chiyoda Ku, Tokyo 1020075, Japan
[3] Tohoku Univ, Grad Sch Engn, Dept Appl Chem, Aoba Ku, Sendai, Miyagi 9808579, Japan
[4] Natl Inst Radiol Sci, Mol Imaging Ctr, Inage Ku, Chiba 2638555, Japan
[5] High Energy Accelerator Res Org, Inst Mat Struct Sci, Tsukuba, Ibaraki 3050801, Japan
来源：
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2009年 / 65卷
基金：
日本科学技术振兴机构;
关键词：
CRYSTAL;
D O I：
10.1107/S160053680903712X
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
Crystals of the title compound, {(C6H5C2H4NH3)(2)[PbBr4]}(n), were grown at room temperature from a solution in N,N-dimethylformamide (DMF) using nitromethane as the poor solvent. This perovskite-type organic-inorganic hybrid compound consists of well ordered sheets of corner-sharing disordered PbBr6 octahedra separated by bilayers of phenethylammonium cations. The octahedra are rotated and tilted due to N-H center dot center dot center dot Br hydrogen bonds with the ammonium groups, generating a superstructure in the unit cell similar to that of the tetrachloridoplumbate (C6H5C2H4NH3)(2)[PbCl4].
引用
收藏
页码：M1323 / U778
页数：21
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