Poly[bis(phenethylammonium) [dibromidoplumbate(II)]-di-μ-bromido]]

被引：53

作者：

Shibuya, Kengo ^{[1
,2
]}

Koshimizu, Masanori ^{[2
,3
]}

Nishikido, Fumihiko ^{[2
,4
]}

Saito, Haruo ^{[1
,2
]}

Kishimoto, Shunji ^{[2
,5
]}

机构：

[1] Univ Tokyo, Grad Sch Arts & Sci, Inst Phys, Meguro Ku, Tokyo 1538902, Japan

[2] Japan Sci & Technol Agcy, CREST, Chiyoda Ku, Tokyo 1020075, Japan

[3] Tohoku Univ, Grad Sch Engn, Dept Appl Chem, Aoba Ku, Sendai, Miyagi 9808579, Japan

[4] Natl Inst Radiol Sci, Mol Imaging Ctr, Inage Ku, Chiba 2638555, Japan

[5] High Energy Accelerator Res Org, Inst Mat Struct Sci, Tsukuba, Ibaraki 3050801, Japan

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2009年 / 65卷

基金：

日本科学技术振兴机构;

关键词：

CRYSTAL;

D O I：

10.1107/S160053680903712X

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

Crystals of the title compound, {(C6H5C2H4NH3)(2)[PbBr4]}(n), were grown at room temperature from a solution in N,N-dimethylformamide (DMF) using nitromethane as the poor solvent. This perovskite-type organic-inorganic hybrid compound consists of well ordered sheets of corner-sharing disordered PbBr6 octahedra separated by bilayers of phenethylammonium cations. The octahedra are rotated and tilted due to N-H center dot center dot center dot Br hydrogen bonds with the ammonium groups, generating a superstructure in the unit cell similar to that of the tetrachloridoplumbate (C6H5C2H4NH3)(2)[PbCl4].

引用

页码：M1323 / U778

页数：21

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