Imaging defects and junctions in single-walled carbon nanotubes by voltage-contrast scanning electron microscopy

被引:19
|
作者
Vijayaraghavan, Aravind [1 ]
Marquardt, Christoph W. [1 ,2 ]
Dehm, Simone [1 ]
Hennrich, Frank [1 ]
Krupke, Ralph [1 ,3 ]
机构
[1] KIT, Inst Nanotechnol, D-76021 Karlsruhe, Germany
[2] KIT, Inst Phys, D-76021 Karlsruhe, Germany
[3] KIT, DFG Ctr Funct Nanostruct CFN, D-76021 Karlsruhe, Germany
关键词
SPECTROSCOPY; TRANSISTORS; TRANSITION;
D O I
10.1016/j.carbon.2009.09.067
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
Voltage-contrast scanning electron microscopy is demonstrated as a new technique to locate and characterize defects in single-walled carbon nanotubes. This method images the surface potential along and surrounding a nanotube in device configuration and it is used here to study the following: (a) structural point-defects formed during nanotube growth, (b) nano-scale gap formed by high-current electrical breakdown, (c) electronic defect such as electron-irradiation induced metal-insulator transition, and (d) charge injection into the substrate which causes hysteresis in nanotube devices. The in situ characterization of defect healing under high bias is also shown. The origin of voltage-contrast, the influence of the above defects on the contrast profiles and optimum imaging conditions are discussed. (C) 2009 Elsevier Ltd. All rights reserved.
引用
收藏
页码:494 / 500
页数:7
相关论文
共 50 条
  • [21] Ultrafast voltage-contrast scanning probe microscopy
    Stanford Univ, Stanford, United States
    Nanotechnology, 4 (385-389):
  • [22] Performing current versus voltage measurements of single-walled carbon nanotubes using scanning force microscopy
    de Pablo, PJ
    Gómez-Navarro, C
    Martínez, MT
    Benito, AM
    Maser, WK
    Colchero, J
    Gómez-Herrero, J
    Baró, AM
    APPLIED PHYSICS LETTERS, 2002, 80 (08) : 1462 - 1464
  • [23] Improved synthesis of carbon nanotubes with junctions and of single-walled carbon nanotubes
    F. L. Deepak
    A. Govindaraj
    C. N. R. Rao
    Journal of Chemical Sciences, 2006, 118 : 9 - 14
  • [24] Improved synthesis of carbon nanotubes with junctions and of single-walled carbon nanotubes
    Deepak, FL
    Govindaraj, A
    Rao, CNR
    JOURNAL OF CHEMICAL SCIENCES, 2006, 118 (01) : 9 - 14
  • [25] Thermal decomposition and electron microscopy studies of single-walled carbon nanotubes
    A. W. Musumeci
    G. G. Silva
    W. N. Martens
    E. R. Waclawik
    R. L. Frost
    Journal of Thermal Analysis and Calorimetry, 2007, 88 : 885 - 891
  • [26] Thermal decomposition and electron microscopy studies of single-walled carbon nanotubes
    Musumeci, A. W.
    Silva, G. G.
    Martens, W. N.
    Waclawik, E. R.
    Frost, R. L.
    JOURNAL OF THERMAL ANALYSIS AND CALORIMETRY, 2007, 88 (03) : 885 - 891
  • [27] In situ scanning electron microscopy of single-walled carbon nanotube growth
    Takagi, Daisuke
    Homma, Yoshikazu
    Suzuki, Satoru
    Kobayashi, Yoshihiro
    SURFACE AND INTERFACE ANALYSIS, 2006, 38 (12-13) : 1743 - 1746
  • [28] Identification of Nitrogen Dopants in Single-Walled Carbon Nanotubes by Scanning Tunneling Microscopy
    Tison, Yann
    Lin, Hong
    Lagoute, Jerome
    Repain, Vincent
    Chacon, Cyril
    Girard, Yann
    Rousset, Sylvie
    Henrard, Luc
    Zheng, Bing
    Susi, Toma
    Kauppinen, Esko I.
    Ducastelle, Francois
    Loiseau, Annick
    ACS NANO, 2013, 7 (08) : 7219 - 7226
  • [29] Observation of elastic deformations in single-walled carbon nanotubes by scanning tunneling microscopy
    Clauss, W
    Bergeron, DJ
    Johnson, AT
    ELECTRONIC PROPERTIES OF NOVEL MATERIALS - PROGRESS IN MOLECULAR NANOSTRUCTURES: XII INTERNATIONAL WINTERSCHOOL, 1998, 442 : 92 - 96
  • [30] Molecular junctions by joining single-walled carbon nanotubes
    Terrones, M
    Banhart, F
    Grobert, N
    Charlier, JC
    Terrones, H
    Ajayan, PM
    PHYSICAL REVIEW LETTERS, 2002, 89 (07) : 1 - 075505