Synthesis, characterization and coordination chemistry of substituted β-amino dicarbonyls

被引：3

作者：

Meskini, Ihssan ^{[2
]}

Daoudi, Maria ^{[2
]}

Kerbal, Abdelali ^{[2
]}

Bennani, Brahim ^{[2
]}

Sheikh, Javed ^{[1
]}

Parvez, Ali ^{[3
]}

Toupet, Loic ^{[4
]}

Ben Hadda, Taibi ^{[5
]}

机构：

[1] Natl Environm Engn Res Inst, Nagpur 440020, Maharashtra, India

[2] Fac Sci Dhar Mehraz, Chim Organ Lab, Fes, Morocco

[3] Rashtrasant Tukadoji Maharaj Nagpur Univ, Dept Chem, Nagpur, Maharashtra, India

[4] Univ Rennes 1, CNRS, UMR 6251, Inst Phys,IPR, Rennes, France

[5] Univ Mohamed Premier, Lab Chim Mat, Oujda, Morocco

来源：

JOURNAL OF SAUDI CHEMICAL SOCIETY | 2012年 / 16卷 / 02期

关键词：

beta-Amino dicarbonyls; Michael reaction; Crystallography; ALPHA; BETA-UNSATURATED CARBONYL-COMPOUNDS; VIRUS TYPE-1 INTEGRASE; ACID METAL-COMPLEXES; AZA-MICHAEL REACTION; HIV-1; INTEGRASE; INHIBITORS; DESIGN; LIGAND;

D O I：

10.1016/j.jscs.2010.12.005

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

An efficient and facile method for the synthesis of novel structurally diverse beta-amino dicarbonyl compounds is described by exploring the aza-Michael addition reaction in an aqueous medium as a key step. Thereby, 2-(aryl-disubstituted-amino-1-yl-methyl)-malonic acid diethyl esters were achieved in a good to excellent yields. These products were easily isolated with enough purity just by using simple recrystallization. The crystals of the compounds (17) and (24) have been obtained and studied by X-ray crystallographic analyses. (C) 2011 King Saud University. Production and hosting by Elsevier B.V. All rights reserved.

引用

页码：161 / 173

页数：13

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