4-(4-Nitrophenyl)-2,3,3a,4,5,9b-hexahydrofuro[3,2-c]quinoline

被引:1
|
作者
Ravikumar, K [1 ]
Sridhar, B
Mahesh, M
Reddy, VVN
机构
[1] Indian Inst Chem Technol, Lab Xray Crystallog, Hyderabad 500007, Andhra Pradesh, India
[2] Indian Inst Chem Technol, Organ Chem Div 2, Hyderabad 500007, Andhra Pradesh, India
关键词
D O I
10.1107/S160053680501175X
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
The title compound, C17H16N2O3, is one of the diastereoisomers formed as the result of the Diels-Alder reaction of 1-(4-nitrophenyl)methylidene]-N-phenylamine and dihydrofuran catalyzed by zirconium tetrachloride. The furan ring adopts an envelope conformation, while the N-heterocyclic ring prefers a sofa conformation. Molecules are linked into centrosymmetric dimers by N-H center dot center dot center dot O hydrogen-bond interactions.
引用
收藏
页码:O1419 / O1421
页数:3
相关论文
共 50 条
  • [31] Synthesis and biological activity of n-acyl-4-phenyl-1,2-epoxy-2,3,3a,4,5,9b-hexahydro-1h-cyclopenta[c]quinolines
    Krainova, G. F.
    Anikina, L. V.
    Vikharev, Yu. B.
    Glushkov, V. A.
    PHARMACEUTICAL CHEMISTRY JOURNAL, 2012, 45 (12) : 712 - 716
  • [32] Behavior of hydrazonoyl chlorides towards the C=N double bond of Δ2-pyrazolines.: A study on 2-(4-nitrophenyl)-2,3,3a,4,5,6-hexahydro-6-oxofuro[3,4-c]pyrazole
    Molteni, G
    Garanti, L
    HETEROCYCLES, 2001, 55 (08) : 1573 - 1580
  • [33] 3-(4-Bromophenyl)-4-[2-(4-nitrophenyl)hydrazinyl]furan-2(5H)-one
    Xiao, Zhu-Ping
    Yi, Li-Cheng
    Li, Jia-Liang
    Zhang, Bo
    Liao, Mei-Ling
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : O3086 - U1857
  • [34] DERIVATIVES OF 2-DICHLOROMETHYL-4-METHYL-2,3-DIHYDROFURO[3,2-C]QUINOLINE
    GYULBUDAGYAN, LV
    SAGATELY.SA
    KHIMIYA GETEROTSIKLICHESKIKH SOEDINENII, 1973, (01): : 84 - 86
  • [35] Furopyridines.: XXIX.: Reactions of furo[2,3-b:4,5-c′]-, -[3,2-b:4,5-c′]-, -[2,3-c:4,5-c′]- and -[3,2-c:3,2-c′]dipyridine
    Yamaguchi, S
    Orito, K
    Shimizu, N
    Taniguchi, K
    Saitoh, H
    Kurosaki, M
    Yokoyama, H
    Hirai, Y
    Shiotani, S
    JOURNAL OF HETEROCYCLIC CHEMISTRY, 1999, 36 (01) : 81 - 94
  • [36] Synthesis, Crystal Structure and Anti-tumor Activity of 2-(2-Chloro-4-nitrophenyl)-4-(4-chlorophenyl)-3a,4-diethoxy-2,3,3a, 4-tetrahydrochromeno[3,4-d][1,2,3]diazaphosphole
    Ying Hua-Zhou
    Sun Mao-Tang
    Liu Tao
    Hu Yong-Zhou
    CHINESE JOURNAL OF STRUCTURAL CHEMISTRY, 2008, 27 (10) : 1171 - 1174
  • [37] Synthesis,Crystal Structure and Anti-tumor Activity of 2-(2-Chloro-4-nitrophenyl)-4-(4-chlorophenyl)-3a,4-diethoxy-2,3,3a,4-tetrahydrochromeno[3,4-d][1,2,3]diazaphosphole
    应华洲
    孙茂堂
    刘滔
    胡永洲
    结构化学, 2008, (10) : 1171 - 1174
  • [38] N-Trifluoroacetyl-3a,4,5,9b-tetrahydro-3H-cyclopenta[c]quinoline ozonides
    A. G. Tolstikov
    R. G. Savchenko
    D. V. Nedopekin
    S. R. Afon’kina
    E. S. Lukina
    V. N. Odinokov
    Russian Chemical Bulletin, 2011, 60 : 160 - 167
  • [39] A convenient synthesis of benzofuro[3,2-c]isoquinolines and naphtho[1′,2′:4,5]furo[3,2-c]isoquinolines
    Kalugin, Victor E.
    Shestopalov, Anatoly M.
    TETRAHEDRON LETTERS, 2011, 52 (14) : 1557 - 1560
  • [40] (4R)-Ethyl 4-(4-chlorophenyl)-2-hydroxy-5-oxo-2,3,4,5-tetrahydropyrano[3,2-c]chromene-2-carboxylate
    Wang, Yifeng
    Zhang, Wei
    Xu, Xiangsheng
    Zhang, Guangcun
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : O217 - U2974