Synthesis and structural study of N′-(4,6-diphenylpyrimidin-2-yl)-2-methylpropanoic hydrazide

被引：0
|
作者：
Rezinskikh, Z. G.
Slepukhin, P. A.
Pervova, I. G.
Lipunova, G. N.
Maslakova, T. I.
Lipunov, I. N.
机构：
[1] Ural State Univ Forestry Engn, Ekaterinburg 620100, Russia
[2] Russian Acad Sci, Inst Organ Synth, Ural Div, Ekaterinburg, Russia
[3] Ural State Tech Univ, Ekaterinburg, Russia
来源：
RUSSIAN JOURNAL OF GENERAL CHEMISTRY | 2007年 / 77卷 / 08期
基金：
俄罗斯基础研究基金会;
关键词：
General Chemistry; Hydrazide; Nickel Nitrate; Pyrimidinyl; Hydrazinyl;
D O I：
10.1134/S107036320708021X
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
Reaction of 1-(4-methoxyphenyl)-3-isopropyl-5-(4,6-diphenylpyrimidin-2-yl)formazan with nickel nitrate in acid medium yields N'-(4,6-diphenylpyrimidin-2-yl)-2-methylpropanoic hydrazide. Its crystal and molecular structure is studied by single crystal X-ray diffraction.
引用
收藏
页码：1422 / 1425
页数：4
相关论文
共 50 条
  • [21] N-(4,6-DIMETHYLPYRIDINE-2-YL)(1-METHYLINDOL-2-YL)CARBOXAMIDE
    RODIER, PN
    CENSE, JM
    ROBERT, JM
    LEBAUT, G
    ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 1992, 48 : 1148 - 1150
  • [22] Design, synthesis, and biological evaluation of polyphenols with 4,6-diphenylpyrimidin-2-amine derivatives for inhibition of Aurora kinase A
    Young Han Lee
    Jihyun Park
    Seunghyun Ahn
    Youngshim Lee
    Junho Lee
    Soon Young Shin
    Dongsoo Koh
    Yoongho Lim
    DARU Journal of Pharmaceutical Sciences, 2019, 27 : 265 - 281
  • [23] N-2-(4,6-DIMETHYLPYRID-2-YL)-N-1-METHYLPYRAZINE-2-CARBOXAMIDINE
    RODIER, N
    RIDEAU, O
    ROBERT, JM
    LEBAUT, G
    ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 1994, 50 : 1760 - 1762
  • [24] Design, synthesis, and biological activities of 3-((4,6-diphenylpyrimidin-2-ylamino) methylene)-2,3-dihydrochromen-4-ones
    Shin, Soon Young
    Jung, Euitaek
    Yeo, Hyunjin
    Ahn, Seunghyun
    Lee, Youngshim
    Park, Jihyun
    Kang, Hyunook
    Yeo, Woon-Seok
    Koh, Dongsoo
    Lim, Yoongho
    BIOORGANIC CHEMISTRY, 2022, 120
  • [25] Design, synthesis, and biological evaluation of polyphenols with 4,6-diphenylpyrimidin-2-amine derivatives for inhibition of Aurora kinase A
    Lee, Young Han
    Park, Jihyun
    Ahn, Seunghyun
    Lee, Youngshim
    Lee, Junho
    Shin, Soon Young
    Koh, Dongsoo
    Lim, Yoongho
    DARU-JOURNAL OF PHARMACEUTICAL SCIENCES, 2019, 27 (01) : 265 - 281
  • [26] Design, Synthesis and Spectral Characterization of Novel 2-morpholino-N-(4,6-diarylpyrimidin-2-yl) acetamides
    Kanagarajan, Vijayakumar
    Thanusu, Jayaraman
    Gopalakrishnan, Mannathusamy
    JOURNAL OF THE KOREAN CHEMICAL SOCIETY-DAEHAN HWAHAK HOE JEE, 2010, 54 (01): : 49 - 54
  • [27] N-(2,6-Difluorobenzoyl)-N′-(4,6-dimethoxypyrimidin-2-yl)urea
    Wang, Qing-Dong
    Xue, Si-Jia
    Yan, Lin
    Ke, Shao-Yong
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2006, 62 : O2824 - O2825
  • [28] Crystal structures and Hirshfeld surface analyses of 2-[(4,6-diaminopyrimidin-2-yl)sulfanyl]-N-(pyridin-2-yl)acetamide and 2-[(4,6-diaminopyrimidin-2-yl)-sulfanyl]-N-(pyrazin-2-yl)acetamide
    Choudhury, Manisha
    Viswanathan, Vijayan
    Timiri, Ajay Kumar
    Sinha, Karij Nayan
    Jayaprakash, Venkatesan
    Velmurugan, Devadasan
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2018, 74 : 718 - +
  • [29] ABINITIO STUDIES OF STRUCTURAL FEATURES NOT EASILY AMENABLE TO EXPERIMENT .38. STRUCTURAL AND CONFORMATIONAL INVESTIGATIONS OF PROPANOIC, 2-METHYLPROPANOIC, AND BUTANOIC ACID
    SIAM, K
    KLIMKOWSKI, VJ
    EWBANK, JD
    SCHAFER, L
    VANALSENOY, C
    JOURNAL OF COMPUTATIONAL CHEMISTRY, 1984, 5 (05) : 451 - 456
  • [30] Synthesis of N-(4,6-dimethylpyridin-2-yl)-benzoxazolinonyl methylcarboxamides with potential antiinflammatory activity
    Liacha, M
    Yous, S
    Depreux, P
    Poupaert, JH
    Lesieur, D
    HETEROCYCLES, 1999, 51 (08) : 1929 - 1943
12345