Structure of molybdenum trioxide prepared from MoO3•H2O

被引：0
|
作者：
Gurlo, AC [1 ]
Ivanovskaya, MI [1 ]
机构：
[1] Belarusian State Univ, Res Inst Physicochem Problems, Minsk 220080, BELARUS
来源：
INORGANIC MATERIALS | 1998年 / 34卷 / 12期
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D O I：
暂无
中图分类号：
T [工业技术];
学科分类号：
08 ;
摘要：
As evidenced by x-ray diffraction, thermal analysis, and IR spectroscopy data, dehydration (air, 200 degrees C) of the hydrous molybdenum trioxide precipitated by adding nitric acid to a solution of (NH4)(6)Mo7O24 yields a hexagonal phase (a = 10.576(4) Angstrom, c = 3.728(4) Angstrom) containing ammonium ions. Calcination of this phase at temperatures between 300 and 400 degrees C yields orthorhombic molybdenum trioxide free of foreign ions.
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页码：1237 / 1239
页数：3
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