A low-cost, environment-friendly and solvent-free route for synthesis of AgBr nanoparticles

被引：3
|
作者：
Shahsavani, Ensieh [1 ]
Dehno Khalaji, Aliakbar [2 ]
Feizi, Nourollah [1 ]
Das, Debasis [3 ]
Sanmartin Matalobos, Jesus [4 ]
Kucerakova, Monika [5 ]
Dusek, Michal [5 ]
机构：
[1] Payame Noor Univ, Dept Chem, Mashhad, Iran
[2] Golestan Univ, Dept Chem, Fac Sci, Gorgan, Iran
[3] Univ Burdwan, Dept Chem, Burdwan 713104, W Bengal, India
[4] Fac Quim, Dept Quim Inorgan, Santiago De Compostela 15782, Spain
[5] Inst Phys ASCR, Vvi, Prague 18221 8, Czech Republic
来源：
SUPERLATTICES AND MICROSTRUCTURES | 2015年 / 82卷
关键词：
AgBr; Nanoparticles; Thiosemicarbazone; XRD; SEM; TEM; THIOSEMICARBAZONE COMPLEX; AGCL NANOPARTICLES; CRYSTAL-STRUCTURES; PRECURSOR; NANOSTRUCTURES; COMPOSITES; COMPOUND; ZINC;
D O I：
10.1016/j.spmi.2015.01.030
中图分类号：
O469 [凝聚态物理学];
学科分类号：
070205 ;
摘要：
We report on the synthesis of AgBr nanoparticles average size below 20 nm by from AgNO3 and a thiosemicarbazone ligand, Brcatsc [Brcatsc = 2-bromo-3-phenylpropenalthiosemicarbazone]. Brcatsc was prepared by reacting alpha-bromocinnam-aldehyde and thiosemicarbazide (1:1, molar ratio) in hot ethanol characterized by elemental analyses (CHN), FT-IR, H-1 NMR spectroscopy and single crystal X-ray diffraction. AgBr nanoparticles were prepared by heating the mixture of AgNO3 and Brcatsc at 600 degrees C for 3 h under aerobic condition, and characterized by X-ray powder diffraction (XRD), scanning electron microscopy (SEM) and transmission electron microscopy (TEM). The XRD pattern clearly indicates the formation of AgBr nanoparticles while SEM and TEM results reveal their uniformity and purity. (C) 2015 Elsevier Ltd. All rights reserved.
引用
收藏
页码：18 / 25
页数：8
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