Sinusoidal ribbon waves in the crystal structure of bis(4-aminophenyl)disulfide

被引：0

作者：

Vittal, JJ ^{[1
]}

Anjali, KS ^{[1
]}

机构：

[1] Natl Univ Singapore, Dept Chem, Singapore 119260, Singapore

来源：

MATERIALS RESEARCH BULLETIN | 1998年

关键词：

organic compounds; X-ray diffraction; crystal structure; hydrogen bonding; crystal engineering;

D O I：

暂无

中图分类号：

T [工业技术];

学科分类号：

08 ;

摘要：

The crystal structure of the compound bis(4-aminophenyl)disulfide was determined by single crystal X-ray crystallography. The S-S distance is 2.074(1) Angstrom, and the S-S-C angles are 104.5(1) and 104.7(1)degrees, respectively. The C-SS-C torsion angle is 80.2(1)degrees. In the crystal structure, the disulfide molecules are connected head-to-tail by weak N-H ... N hydrogen bonding to form a polymeric chain and two such strands are linked by N-H ... S bonding (S ... H distance, 2.79(2) Angstrom) to look like sinusoidal ribbon waves when viewed down the c-axis. The N ... N and N ... H distances are 3.160(4) and 2.36(2) Angstrom, respectively. (C) 1998 Elsevier Science Ltd.

引用

页码：147 / 152

页数：6

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