Dynamic microstructure evolution and mechanical properties of dilute Mg-Al-Ca-Mn alloy during hot rolling

The dynamic microstructure and texture of dilute Mg-0.50Al-0.71Ca-0.33Mn (wt.%) during hot rolling at two slab temperatures were investigated by electron backscattered diffraction (EBSD) and high resolution transmission electron microscopy (HRTEM). The results show that the development of the rolling microstructures is to first form {10-12} extension twins in the original grains, thereby forming the extension-twinned regions, and then to further form {10-11} -{10-12} double twins and kinks in the extension-twinned regions, and finally to form continuous dynamic recrystallized (continuous DRXed) grains in the double twins and the cross parts of the shear-deformed coarse extension-twinned regions. These extension twins, double twins and kinks show a decisive effect on the formation of rolling texture. The number of {10-11} -{10-12} double twins and resultant the continuous DRX process are strongly affected by the rolling slab temperature and the reduction thickness per pass. By optimizing the rolling conditions, texture and microstructures of the multi-pass rolled Mg-Al-Ca-Mn alloy sheets are successfully modified. Although the total alloy content is only 1.5 wt.%, these Mg-Al-Ca-Mn alloy sheets show much higher strength than the commercial Mg-3Al-1 Zn (wt.%) (AZ31B) sheet. (c) 2022 Published by Elsevier Ltd on behalf of The editorial office of Journal of Materials Science & Technology.