Syntheses, Crystal Structures and Properties of Two New Compounds from a Flexible Bipodal Acid with Additional Amide Groups

被引：2

作者：

Xu Han ^{[1
,2
]}

Zheng He-Gen ^{[2
]}

机构：

[1] Huangshan Univ, Sch Chem & Chem Engn, Huangshan 245041, Anhui, Peoples R China

[2] Nanjing Univ, Sch Chem & Chem Engn, Nanjing 210093, Jiangsu, Peoples R China

来源：

CHINESE JOURNAL OF STRUCTURAL CHEMISTRY | 2017年 / 36卷 / 06期

基金：

中国国家自然科学基金;

关键词：

magnetic properties; reversible crystal-to-amorphous; bipodal flexible ligand; COORDINATION POLYMERS; MAGNETIC-PROPERTIES; ORGANIC FRAMEWORK; COMPLEXES; TOPOLOGY; LIGANDS; WATER;

D O I：

10.14102/j.cnki.0254-5861.2011-1460

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

Two novel compounds {[Cu(IBG)(4,4'-bipy)(H2O)(2)](2)center dot 11H(2)O}(n)(1) and {[Co(IBG)(mu-H2O)(H2O)(2)]center dot 2H(2)O}(n)(2) based on isophthaloylbisglycine (H(2)IBG) have been synthesized and structurally characterized by thermogravimetric analysis, elemental analysis and single-crystal X-ray diffraction. Compound 1 shows a 1D chain sine/cosine chain structure, and compound 2 can be characterized as a 4-connected sql tetragonal planar network with the point symbol of {4(4)center dot 6(2)}. Compound 2 has been characterized by magnetic measurements. In addition, 1 and 2 display an interesting reversible crystal-to-amorphous transformation.

引用

页码：1034 / 1042

页数：9

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