Synthesis, Optimization and Characterization of Silicon Carbide (SiC) from Rice Husk

被引:23
|
作者
Alweendo, Shatumbu T. [1 ]
Johnson, Oluwagbenga T. [1 ]
Shongwe, Mxolisi B. [2 ]
Kavishe, Frank P. L. [1 ]
Borode, Joseph O. [3 ]
机构
[1] Univ Namibia, Dept Min & Met Engn, Ongwediva, Namibia
[2] Tshwane Univ Technol, Inst Nano Engn Res, Dept Chem Met & Mat Engn, Pretoria, South Africa
[3] Fed Univ Technol Akure, Dept Met & Mat Engn, Akure, Nigeria
关键词
Silicon carbide; Rice husk; pyrolysis; carbothermal reduction; PYROLYSIS; WASTE;
D O I
10.1016/j.promfg.2019.06.042
中图分类号
X [环境科学、安全科学];
学科分类号
08 ; 0830 ;
摘要
Although Silicon carbide (SiC) has shown interesting engineering properties, its cost of production continues to limit its applications in the industry. Therefore, this paper reports a simple, inexpensive method to synthesize silicon carbide via pyrolysis of rice husk without the use of catalysts or complex set-ups. Pyrolysis of rice husk was carried out in a tube furnace at temperatures ranging from 1000 degrees C to 1500 degrees C and retention time ranging from 1 to 2 hours in an Argon atmosphere flowing at a rate of 21/min. The morphology of the products was analysed by SEM while phase analysis was done using XRD. The yield of SiC from rice husk was found to be affected significantly by pyrolysis temperature and retention time. It was observed that the synthesized SiC powder was a mixture of whiskers and particulates. (C) 2019 The Authors. Published by Elsevier B.V.
引用
收藏
页码:962 / 967
页数:6
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