Structural and spectroscopic characterization of N,N′-bis(2-pyridylmethyl)-ethylenediamine tetrahydrochloride dihydrate

被引：3

作者：

Zinczuk, J. ^{[4
]}

Echeverria, G. A. ^{[2
,3
]}

Piro, O. E. ^{[2
,3
]}

Parajon-Costa, B. S. ^{[1
]}

Baran, E. J. ^{[1
]}

机构：

[1] Natl Univ La Plata, Fac Ciencias Exactas, CONICET UNLP, Ctr Quim Inorgan CEQUINOR, RA-1900 La Plata, Argentina

[2] Natl Univ La Plata, Fac Ciencias Exactas, Dept Fis, RA-1900 La Plata, Argentina

[3] Natl Univ La Plata, Fac Ciencias Exactas, Inst IFLP CONICET, RA-1900 La Plata, Argentina

[4] Univ Nacl Rosario, Fac Ciencias Bioquim & Farmaceut, UNR, Inst Quim Rosario IQUIR CONICET, RA-2000 Rosario, Santa Fe, Argentina

来源：

JOURNAL OF MOLECULAR STRUCTURE | 2011年 / 994卷 / 1-3期

关键词：

N; N '-bis(2-pyridylmethyl)-ethylenediamine tetrahydrochloride dihydrate; Crystal structure; IR spectra; Raman spectra; NMR spectra; COMPLEXES; LIGAND; MONONUCLEAR; BISPICEN;

D O I：

10.1016/j.molstruc.2011.03.038

中图分类号：

O64 [物理化学（理论化学）、化学物理学];

学科分类号：

070304 ; 081704 ;

摘要：

The crystal structure of the title compound, [(C(5)H(4)NH)-CH(2)-NH(2)-(CH(2))(2)-NH(2)-CH(2)(C(5)H(4)NH)]Cl(4)center dot 2H(2)O, a potentially useful agent for chelation therapies, has been determined by single crystal X-ray diffractometry. It crystallizes in the monoclinic space group P2(1)/c with Z = 2. The FT-IR and Raman spectra as well as the (1)H and (13)C NMR spectra of the compound were also recorded and briefly discussed. (c) 2011 Elsevier B.V. All rights reserved.

引用

页码：302 / 305

页数：4

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