A Novel Sample Pretreatment Method for the Analysis of Polybrominated Diphenyl Ethers in Polymers of Waste Electrical and Electronic Equipment (WEEE)

被引：5

作者：

Huang, Fan ^{[1
]}

Meng, Xiangzhou ^{[1
]}

Chen, Ling ^{[1
]}

Xiang, Nan ^{[1
]}

Liu, Ying ^{[1
]}

Li, Guangming ^{[1
]}

机构：

[1] Tongji Univ, Coll Environm Sci & Engn, State Key Lab Pollut Control & Resources Reuse, Shanghai 200092, Peoples R China

来源：

CHINESE JOURNAL OF CHEMISTRY | 2010年 / 28卷 / 08期

基金：

中国国家自然科学基金;

关键词：

PBDEs; polymers; WEEE; film; Soxtec extraction; BROMINATED FLAME RETARDANTS; STYRENIC POLYMERS; EXTRACTION; EXPOSURE; IDENTIFICATION; CHROMATOGRAPHY;

D O I：

10.1002/cjoc.201090252

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

A fast sample pretreatment method was developed to determine polybrominated diphenyl ethers (PBDEs) in polymers from waste electrical and electronic equipment (WEEE). Polymers were firstly prepared into "polymer film" to facilitate a complete Soxtec extraction. Then, three extraction parameters (including hot plate temperature, boiling time, and rinsing time) were optimized based on the recovery of target in reference polymer samples. The proposed method was successfully applied to the analysis of PBDEs in standard plastic materials from WEEE and the extraction yields of PBDEs ranged from 78.9% to 91.3%. The detection limits of PBDEs were 0.05-0.10 mu g/g, indicating this method can be used as a quality assurance and quality control procedure of PBDEs in the production of electrical and electronic equipment.

引用

页码：1475 / 1481

页数：7

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