Synthesis of the first dithiaaza-17-crown-5 ethers containing piperidin-4-one subunit

被引：0
|
作者：
Thi, Thanh Van Tran [1 ]
Nguyen, Manh Linh [1 ,2 ]
Nguyen, Tien Dat [1 ]
Le, The Duan [1 ]
Truong, Hong Hieu [3 ]
Khrustalev, Victor N. [3 ,4 ]
Le, Tuan Anh [1 ]
机构：
[1] Vietnam Natl Univ, VNU Univ Sci, Fac Chem, 334 Nguyen Trai St, Hanoi 100000, Vietnam
[2] Thai Nguyen Univ Med & Pharm, Fac Pharm, 284 Luong Ngoc Quyen St, Thai Nguyen City 250000, Vietnam
[3] RUDN Univ, 6 Miklukho Maklaya St, Moscow 117198, Russia
[4] Russian Acad Sci, ND Zelinsky Inst Organ Chem, 47 Leninsky Ave, Moscow 119991, Russia
来源：
CHEMISTRY OF HETEROCYCLIC COMPOUNDS | 2021年 / 57卷 / 10期
关键词：
dithiaaza-17-crown-5; ether; 2,2 '-[ethane-1,2-diylbis(oxyethane-2,1-diylsulfanediyl)]dibenzaldehyde; domino reaction; Petrenko-Kritschenko reaction; MOLECULAR-STRUCTURE; CRYSTAL;
D O I：
10.1007/s10593-021-03022-1
中图分类号：
O62 [有机化学];
学科分类号：
070303 ; 081704 ;
摘要：
Dithiaaza-17-crown-5 ethers containing piperidin-4-one subunit and dithiacrown ether fragment were synthesized in one-pot Petrenko-Kritschenko reaction from 2,2'-[ethane-1,2-diylbis(oxyethane-2,1-diylsulfanediyl)]dibenzaldehyde, methyl ethyl ketone or dibenzyl ketone, and ammonium acetate. Molecular structure of dithiaaza-17-crown-5 ethers were confirmed by NMR, HRMS, and single crystal X-ray diffraction.
引用
收藏
页码：1057 / 1060
页数：4
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