Synthesis of the first dithiaaza-17-crown-5 ethers containing piperidin-4-one subunit

被引：0

作者：

Thi, Thanh Van Tran ^{[1
]}

Nguyen, Manh Linh ^{[1
,2
]}

Nguyen, Tien Dat ^{[1
]}

Le, The Duan ^{[1
]}

Truong, Hong Hieu ^{[3
]}

Khrustalev, Victor N. ^{[3
,4
]}

Le, Tuan Anh ^{[1
]}

机构：

[1] Vietnam Natl Univ, VNU Univ Sci, Fac Chem, 334 Nguyen Trai St, Hanoi 100000, Vietnam

[2] Thai Nguyen Univ Med & Pharm, Fac Pharm, 284 Luong Ngoc Quyen St, Thai Nguyen City 250000, Vietnam

[3] RUDN Univ, 6 Miklukho Maklaya St, Moscow 117198, Russia

[4] Russian Acad Sci, ND Zelinsky Inst Organ Chem, 47 Leninsky Ave, Moscow 119991, Russia

来源：

CHEMISTRY OF HETEROCYCLIC COMPOUNDS | 2021年 / 57卷 / 10期

关键词：

dithiaaza-17-crown-5; ether; 2,2 '-[ethane-1,2-diylbis(oxyethane-2,1-diylsulfanediyl)]dibenzaldehyde; domino reaction; Petrenko-Kritschenko reaction; MOLECULAR-STRUCTURE; CRYSTAL;

D O I：

10.1007/s10593-021-03022-1

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

Dithiaaza-17-crown-5 ethers containing piperidin-4-one subunit and dithiacrown ether fragment were synthesized in one-pot Petrenko-Kritschenko reaction from 2,2'-[ethane-1,2-diylbis(oxyethane-2,1-diylsulfanediyl)]dibenzaldehyde, methyl ethyl ketone or dibenzyl ketone, and ammonium acetate. Molecular structure of dithiaaza-17-crown-5 ethers were confirmed by NMR, HRMS, and single crystal X-ray diffraction.

引用

页码：1057 / 1060

页数：4

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