The synthesis of 1,5:3,7-dimethano-1,3,5,7-benzotetrazonine

被引：5
|
作者：
Kuznetsov, A. I. [1 ]
Shukkur, A. H. [1 ]
Kamara, K. [1 ]
机构：
[1] MV Lomonosov Moscow State Acad Fine Chem Technol, Moscow 119571, Russia
来源：
RUSSIAN CHEMICAL BULLETIN | 2007年 / 56卷 / 03期
关键词：
o-phenylenediamine; 1,2-diamino-4-methylbenzene; ammonia; formaldehyde; X-ray diffraction analysis;
D O I：
10.1007/s11172-007-0094-0
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
A three-component condensation of formaldehyde, o-phenylenediamine, and ammonia gave a novel 1,5: 3,7-dimethano-1,3,5,7-benzotetrazonine. Its structure was determined by X-ray diffraction analysis. An analogous condensation of formaldehyde, ammonia, and 1,2-diamino-4-methylbenzene yielded 9-methyl-1,5:3,7-dimethano-1,3,5,7-benzotetrazonine.
引用
收藏
页码：563 / 565
页数：3
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