X-Ray diffraction, differential scanning calorimetry and thermogravimetry combined with infrared analysis of freeze-dried prednisolone hemisuccinate

被引:0
|
作者
Claussen, S [1 ]
Böse, M [1 ]
Dittgen, M [1 ]
机构
[1] Jenapharm GmbH & Co KG, Res & Dev, D-07745 Jena, Germany
来源
PHARMAZIE | 2001年 / 56卷 / 06期
关键词
D O I
暂无
中图分类号
R914 [药物化学];
学科分类号
100701 ;
摘要
In this study, the thermal behaviour of freeze-dried prednisolone hemisuccinate (Prednisolut((R))) was investigated by means of X-ray scattering, differential scanning calorimetry (DSC) and fourier transformation infra-red analysis (FT-IR).
引用
收藏
页码:475 / 476
页数:2
相关论文
共 50 条
  • [41] A simultaneous X-ray diffraction-differential scanning calorimetry study into the phase transitions of mefenamic acid
    Pang, Yuying
    Buanz, Asma
    Telford, Richard
    Magdysyuk, Oxana V.
    Gaisford, Simon
    Williams, Gareth R.
    JOURNAL OF APPLIED CRYSTALLOGRAPHY, 2019, 52 : 1264 - 1270
  • [42] Application of differential scanning calorimetry and X-ray powder diffraction to the solid-state study of metoclopramide
    Pabon, CV
    Frutos, P
    Lastres, JL
    Frutos, G
    JOURNAL OF PHARMACEUTICAL AND BIOMEDICAL ANALYSIS, 1996, 15 (01) : 131 - 138
  • [43] An improved hermetic sample enclosure for simultaneous differential scanning calorimetry/synchrotron powder X-ray diffraction
    Lexa, D
    THERMOCHIMICA ACTA, 2003, 398 (1-2) : 241 - 248
  • [44] Crystallization and x-ray diffraction of crystals formed in water-plasticized amorphous spray-dried and freeze-dried lactose/protein mixtures
    Haque, MK
    Roos, YH
    JOURNAL OF FOOD SCIENCE, 2005, 70 (05) : E359 - E366
  • [45] X-RAY MICROANALYSIS OF ULTRATHIN FROZEN AND FREEZE-DRIED SECTIONS OF HUMAN SPERM CELLS
    CHANDLER, JA
    BATTERSBY, S
    JOURNAL OF MICROSCOPY, 1976, 107 (MAY) : 55 - 65
  • [46] ELECTRON-BEAM X-RAY MICROANALYSIS OF ISOLATED, FREEZE-DRIED GIANT CHROMOSOMES
    TROSCH, W
    LINDEMANN, B
    JOURNAL DE MICROSCOPIE ET DE BIOLOGIE CELLULAIRE, 1975, 22 (2-3): : 487 - 491
  • [47] Multifrequency EPR study on freeze-dried fruits before and after X-ray irradiation
    Yordanov, N. D.
    Aleksieva, K.
    Dimitrova, A.
    Georgieva, L.
    Tzvetkova, E.
    RADIATION PHYSICS AND CHEMISTRY, 2006, 75 (09) : 1069 - 1074
  • [48] Structural and thermal characterization of glyceryl behenate by X-ray diffraction coupled to differential calorimetry and infrared spectroscopy
    Brubach, J. B.
    Jannin, V.
    Mahler, B.
    Bourgaux, C.
    Lessieur, P.
    Roy, P.
    Ollivon, M.
    INTERNATIONAL JOURNAL OF PHARMACEUTICS, 2007, 336 (02) : 248 - 256
  • [49] Differential scanning calorimetry study on thermal behaviors of freeze-dried poly(L-lactide) from dilute solutions
    Sasaki, T
    Yamauchi, N
    Irie, S
    Sakurai, K
    JOURNAL OF POLYMER SCIENCE PART B-POLYMER PHYSICS, 2005, 43 (02) : 115 - 124
  • [50] A new experimental setup for combined fast differential scanning calorimetry and X-ray photon correlation spectroscopy
    Martinelli, Alessandro
    Baglioni, Jacopo
    Sun, Peihao
    Dallari, Francesco
    Pineda, Eloi
    Duan, Yajuan
    Spitzbart-Silberer, Tobias
    Westermeier, Fabian
    Sprung, Michael
    Monaco, Giulio
    JOURNAL OF SYNCHROTRON RADIATION, 2024, 31 : 557 - 565