The synthesis of MCM-48 with high yields

被引：39
|
作者：
Wang, SG [1 ]
Wu, D [1 ]
Sun, YH [1 ]
Zhong, B [1 ]
机构：
[1] Chinese Acad Sci, State Key Lab Coal Convers, Inst Coal Chem, Taiyuan 030001, Peoples R China
来源：
MATERIALS RESEARCH BULLETIN | 2001年 / 36卷 / 09期
基金：
中国国家自然科学基金;
关键词：
nanostructures; chemical synthesis;
D O I：
10.1016/S0025-5408(01)00645-6
中图分类号：
T [工业技术];
学科分类号：
08 ;
摘要：
Using tetraethyl orthosilicate as a silica source and cetyltrimethylammonium bromide as a template, MCM-48 mesoporous molecular sieves were synthesized with hydrothermal methods. Reducing the pH of the solution during synthesis improved the yield of MCM-48 and enhanced its stability. While the pH was adjusted to 5, a high yield of 98% was gained. XRD and N-2 adsorption-desorption isotherms were used to characterize the synthesized samples. These mesoporous molecular sieves showed high specific surface areas and ordered channel systems. (C) 2001 Elsevier Science Ltd. All rights reserved.
引用
收藏
页码：1717 / 1720
页数：4
相关论文
共 50 条
  • [21] Influence of synthesis conditions on structural properties of MCM-48
    Taralkar, U. S.
    Kasture, M. W.
    Joshi, P. N.
    JOURNAL OF PHYSICS AND CHEMISTRY OF SOLIDS, 2008, 69 (08) : 2075 - 2081
  • [22] Effect of processing parameters on the synthesis of mesoporous MCM-48
    Boote, Brett
    Subramanian, Hariharaputhiran
    Ranjit, Koodali T.
    ABSTRACTS OF PAPERS OF THE AMERICAN CHEMICAL SOCIETY, 2007, 233 : 232 - 232
  • [23] Synthesis of pure silica molecular sieves MCM-48
    Zhai, SR
    Pu, M
    Zhang, Y
    Wu, D
    Sun, YH
    CHINESE JOURNAL OF INORGANIC CHEMISTRY, 2002, 18 (11) : 1081 - 1085
  • [24] Synthesis of MCM-48 single crystals with cube morphology
    Kong, LD
    Liu, S
    Yan, XW
    Li, QZ
    He, HY
    CHEMISTRY LETTERS, 2005, 34 (04) : 568 - 569
  • [25] Reproducible synthesis of high quality MCM-48 by extraction and recuperation of the gemini surfactant
    Benjelloun, M
    Van der Voort, P
    Cool, P
    Collart, O
    Vansant, EF
    PHYSICAL CHEMISTRY CHEMICAL PHYSICS, 2001, 3 (01) : 127 - 131
  • [26] Synthesis of High Quality MCM-48 with Binary Cationic-Nonionic Surfactants
    Zhao, Wei
    Li, Quanzhi
    Wang, Lina
    Chu, Jinglong
    Qu, Jinkui
    Li, Shaohua
    Qi, Tao
    LANGMUIR, 2010, 26 (10) : 6982 - 6988
  • [27] Synthesis of MCM-48 by microwave-hydrothermal process
    Bandyopadhyay, A
    Gies, H
    COMPTES RENDUS CHIMIE, 2005, 8 (3-4) : 621 - 626
  • [28] Synthesis and characterization of aluminum-containing MCM-48
    Hartmann, M
    Bischof, C
    MESOPOROUS MOLECULAR SIEVES 1998, 1998, 117 : 249 - 256
  • [29] Simplified description of MCM-48
    Anderson, MW
    ZEOLITES, 1997, 19 (04): : 220 - 227
  • [30] Synthesis of high-quality MCM-48 and MCM-41 by means of the GEMINI surfactant method
    Van der Voort, P
    Mathieu, M
    Mees, F
    Vansant, EF
    JOURNAL OF PHYSICAL CHEMISTRY B, 1998, 102 (44): : 8847 - 8851
12345