Synthesis of a high-energy-capacity compound, tetrammine-cis-bis(nitro-2H-tetrazolato-N2)cobalt(III) perchlorate

被引：30

作者：

Zhilin, AY ^{[1
]}

Ilyushin, MA ^{[1
]}

Tselinskii, IV ^{[1
]}

Brykov, AS ^{[1
]}

机构：

[1] St Petersburg State Technol Inst, St Petersburg, Russia

来源：

RUSSIAN JOURNAL OF APPLIED CHEMISTRY | 2001年 / 74卷 / 01期

关键词：

Inorganic compounds - Microwave heating;

D O I：

10.1023/A:1012756202841

中图分类号：

O69 [应用化学];

学科分类号：

081704 ;

摘要：

The conditions for preparing tetrammine-cis-bis(nitro-2H-tetrazolato-N-2)cobalt(III) perchlorate and the nature of impurities affecting the yield and purity of the target product were studied. The compound can be efficiently prepared using microwave heating.

引用

页码：99 / 102

页数：4

共 40 条

[11] SYNTHETIC ANALOG APPROACH TO COBALT(III) BLEOMYCIN - SYNTHESIS, CRYSTAL AND SOLUTION STRUCTURES AND REDOX PROPERTIES OF BIS(N-(2-(4-IMIDAZOLYL)ETHYL)PYRIMIDINE-4-CARBOXAMIDO)COBALT(III) PERCHLORATE.2.25H2O
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[12] NITRO[2R,8R-1,9-BIS(2-PYRIDYL)-2,5,8-TRIAZANONANE]COBALT(III)PERCHLORATE, [CO(C16H23N5)NO2](CLO4)2
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CRYSTAL STRUCTURE COMMUNICATIONS, 1982, 11 (03): : 1163 - 1168
[13] SYNTHESIS AND STRUCTURE OF BIS[2-[(2-PYRIDYLMETHYL)AMINO]EYHYLSULFINATO]-COBALT(III) PERCHLORATE DIHYDRATE - STRUCTURAL TRANS EFFECT IN CO(III)N4OS OR CO(III)N5S COMPLEXES
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[14] (5-Carboxy-1H-pyrazole-3-carboxylato-κ2N2,O3)bis(1,10-phenanthroline-κ2 N,N′)cobalt(III) perchlorate 2.5-hydrate
Xie, Hui-Dong
Xie, Cheng-Zhi
Wang, Xiao-Qing
Shen, Guang-Qiu
Shen, De-Zhong
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2007, 63 : M1477 - M1479
[15] SYNTHESIS AND CHARACTERIZATION OF THE CHROMIUM(III) DIMER BIS(MU-HYDROXO)BIS[[N,N'-BIS(2-PYRIDYLMETHYL)-1,2-ETHANEDIAMINE]CHROMIUM(III)] PERCHLORATE, [(BISPICEN)CR(OH)]2(CLO4)4.H2O
HEINRICHS, MA
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INORGANIC CHEMISTRY, 1984, 23 (20) : 3174 - 3180
[16] Crystal structure of bis[N-(2-aminopropyl)-salicylaldiminato)]cobalt(III) perchlorate,C20H26ClCoN4O6
Zhu, HL
Liu, WJ
Wang, YF
Wang, DQ
ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2003, 218 (02): : 255 - 256
[17] The synthesis, characterization, and X-ray crystal structure of trans-bis(1,3-diamino-2-propanolato-N,N′,O)- cobalt(III) perchlorate trihydrate
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Journal of Chemical Crystallography, 2003, 33 : 569 - 574
[18] The synthesis, characterization, and X-ray crystal structure of trans-bis(1,3-diamino-2-propanolato-N,N′,O)-cobalt(III) perchlorate trihydrate
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JOURNAL OF CHEMICAL CRYSTALLOGRAPHY, 2003, 33 (07) : 569 - 574
[19] CIS-MER-BIS(N-(2,2-DIACETYLVINYL)-O-PHENYLENEDIAMINE)COBALT(III) IODIDE HYDRATE, [CO(C12H13N2O2)2]I.H2O
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YMEN, I
CRYSTAL STRUCTURE COMMUNICATIONS, 1981, 10 (02): : 423 - 428
[20] An unexpected chelate conformation in trans-[(R)-N,N′-bis(α-phenylsalicylidene)propane-1,2-diaminato(2-)]-bis(1-methyl-1H-imidazole-κN3)-cobalt(III) perchlorate
Hirotsu, M
Kojima, M
Nakajima, K
Kashino, S
Yoshikawa, Y
ACTA CRYSTALLOGRAPHICA SECTION C-STRUCTURAL CHEMISTRY, 2004, 60 : M431 - M432

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