An efficient and facile one-pot synthesis of cyanohydrin esters from carbonyl compounds catalyzed by iron(III) chloride

被引:40
|
作者
Iwanami, K [1 ]
Aoyagi, M [1 ]
Oriyama, T [1 ]
机构
[1] Ibaraki Univ, Fac Sci, Mito, Ibaraki 3108512, Japan
关键词
cyanation; cyanohydrin ester; trimethylsilyl cyanide; acid anhydride; carbonyl compound; iron(III) chloride;
D O I
10.1016/j.tetlet.2005.09.003
中图分类号
O62 [有机化学];
学科分类号
070303 ; 081704 ;
摘要
A variety of cyanohydrin esters were readily prepared from carbonyl compounds with trimethylsilyl cyanide and acid anhydride under the influence of a catalytic amount of iron(III) chloride in a convenient one-pot procedure. (c) 2005 Elsevier Ltd. All rights reserved.
引用
收藏
页码:7487 / 7490
页数:4
相关论文
共 50 条
  • [41] A facile one-pot synthesis of (Z)-α-chloro-α, β-unsaturated esters from alcohols
    Karama, U.
    Alshamari, H.
    Abdelall, H.
    Sultan, M.
    ARABIAN JOURNAL OF CHEMISTRY, 2017, 10 : S1537 - S1540
  • [42] One-Pot Oxidation-Hydrocyanation Sequence Coupled to Lipase-Catalyzed Diastereoresolution in the Chemoenzymatic Synthesis of Sugar Cyanohydrin Esters
    Hietanen, Ari
    Kanerva, Liisa T.
    EUROPEAN JOURNAL OF ORGANIC CHEMISTRY, 2012, 2012 (14) : 2729 - 2737
  • [43] Nickel(II) chloride catalyzed one-pot synthesis of α-aminonitriles
    De, SK
    JOURNAL OF MOLECULAR CATALYSIS A-CHEMICAL, 2005, 225 (02) : 169 - 171
  • [44] Cobalt(II) chloride catalyzed one-pot synthesis of α-aminonitriles
    De, Surya K.
    BEILSTEIN JOURNAL OF ORGANIC CHEMISTRY, 2005, 1
  • [45] Polyaniline/SiO2 Catalyzed One-pot Mannich Reaction: An Efficient Synthesis of beta-amino Carbonyl Compounds
    Yelwande, Ajeet A.
    Arbad, Balasaheb R.
    Lande, Machhindra K.
    JOURNAL OF THE KOREAN CHEMICAL SOCIETY-DAEHAN HWAHAK HOE JEE, 2011, 55 (04): : 644 - 649
  • [46] Chromium(III) chloride catalyzed one-pot synthesis of pyrimidine-2-thiones from arylidines and thioureas
    Moirangthem, Nimalini D.
    Laitonjam, Warjeet S.
    INDIAN JOURNAL OF CHEMISTRY SECTION B-ORGANIC CHEMISTRY INCLUDING MEDICINAL CHEMISTRY, 2009, 48 (07): : 1023 - 1026
  • [47] Facile iron(III) chloride hexahydrate catalyzed synthesis of coumarins
    Prateeptongkum, Saisuree
    Duangdee, Nongnaphat
    Thongyoo, Panumart
    ARKIVOC, 2015, : 248 - 258
  • [48] Samarium(III) Iodide Catalyzed One-Pot Synthesis of α-Aminonitriles
    Wu, Jirong
    Chen, Weifeng
    Luo, Mengxian
    He, Xiaolin
    Li, Zhifang
    CHINESE JOURNAL OF ORGANIC CHEMISTRY, 2010, 30 (10) : 1497 - 1501
  • [49] Lanthanum(III) nitrate hexahydrate or gadolinium(III) chloride hexahydrate catalyzed one-pot synthesis of α-amino nitriles
    Narasimbulu, M.
    Reddy, T. Srikanth
    Mahesh, K. Chinni
    Reddy, S. Malla
    Reddy, A. Vijender
    Venkateswarlu, Y.
    JOURNAL OF MOLECULAR CATALYSIS A-CHEMICAL, 2007, 264 (1-2) : 288 - 292
  • [50] Cobalt carbonyl as an effective CO source in one-pot synthesis of esters from aryl halides
    Baburajan, P.
    Senthilkumaran, R.
    Elango, Kuppanagounder P.
    NEW JOURNAL OF CHEMISTRY, 2013, 37 (10) : 3050 - 3056