Combined cation exchange-liquid-liquid extraction method for GC-MS determination of 4-nonylphenol content in water

被引：0
|
作者：
Cruceru, Ioana [1 ]
Badea, Irinel Adriana [1 ]
Vladescu, Luminita [1 ]
机构：
[1] Univ Bucharest, Fac Chem, Dept Analyt Chem, Bucharest 030018, Romania
来源：
REVISTA DE CHIMIE | 2007年 / 58卷 / 12期
关键词：
4-nonylphenol; cation exchange-liquid-liquid extraction procedure; GC-MS;
D O I：
暂无
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
An efficient and highly selective combined cation exchange-liquid-liquid extraction method coupled with GC-MS determination is proposed for the separation and concentration of 4-nonylphenol from various water matrices. The method has good precision expressed as repeatability: mean value 97.28% with a RSD value of 4.20%. Recovery of alkylphenols from spiked samples varies from 92 to 101% and the values obtained are higher than with other methods currently in use. The method was successfully applied for the determination of 4-nonylphenol from various water matrices.
引用
收藏
页码：1305 / 1309
页数：5
相关论文
共 50 条
  • [21] Fast analysis of 4-tertoctylphenol, pentachlorophenol and 4-nonylphenol in river sediments by QuEChERS extraction procedure combined with GC-QqQ-MS/MS
    Czech, T.
    Barco Bonilla, N.
    Gambus, F.
    Romero Gonzalez, R.
    Marin-Saez, J.
    Martinez Vidal, J. L.
    Garrido Frenich, A.
    SCIENCE OF THE TOTAL ENVIRONMENT, 2016, 557 : 681 - 687
  • [22] Multivariate optimization of dispersive liquid-liquid microextraction for the determination of paclobutrazol and triflumizole in water by GC-MS
    Chormey, Dotse Selali
    Karakus, Yesim
    Karayaka, Sena
    Ozsoyler, Cagla
    Bozdogan, Abdurrezzak Emin
    Bakirdere, Sezgin
    JOURNAL OF SEPARATION SCIENCE, 2017, 40 (23) : 4541 - 4548
  • [23] Improved Homogeneous Liquid–Liquid Extraction Combined with GC–ECD for the Determination of Organochlorinated Pesticides in Water
    Farahnaz Rezaei
    Mohammad-Reza Milani Hosseini
    Chromatographia, 2012, 75 : 379 - 385
  • [24] A Novel Liquid–Liquid Extraction for the Determination of Sertraline in Tap Water and Waste Water at Trace Levels by GC–MS
    Elif Seda Koçoğlu
    Sezgin Bakırdere
    Seyfullah Keyf
    Bulletin of Environmental Contamination and Toxicology, 2017, 99 : 354 - 359
  • [25] Validation of a Method for Analysis of Aroma Compounds in Red Wine using Liquid-Liquid Extraction and GC-MS
    Ivanova, Violeta
    Stefova, Marina
    Stafilov, Trajce
    Vojnoski, Borimir
    Biro, Ildiko
    Bufa, Anita
    Kilar, Ferenc
    FOOD ANALYTICAL METHODS, 2012, 5 (06) : 1427 - 1434
  • [26] Differential Pulse Voltammetric Method for 4-Nonylphenol Determination in Water Samples
    Buleandra, Mihaela
    Rabinca, Andreea Alexandra
    Mitran, Elena Cornelia
    Ciucu, Anton Alexandru
    MATERIALE PLASTICE, 2016, 53 (03) : 491 - 494
  • [27] Determination of phthalate esters in bottled water using dispersive liquid-liquid microextraction coupled with GC-MS
    Mousa, Amayreh
    Basheer, Chanbasha
    Al-Arfaj, Abdul Rahman
    JOURNAL OF SEPARATION SCIENCE, 2013, 36 (12) : 2003 - 2009
  • [28] Speciation analysis of organotin compounds (OTCs) by a simultaneous hydride generation-liquid/liquid extraction and GC-MS determination
    Yanez, Jorge
    Riffo, Paula
    Mansilla, Hector D.
    Bravo, Manuel
    Quiroz, Waldo
    Santander, Paola
    MICROCHEMICAL JOURNAL, 2016, 126 : 460 - 465
  • [29] Determination of fenazaquin in water and tomato matrices by GC-MS after a combined QuEChERS and switchable solvent liquid phase microextraction
    Turan, Nouha Bakaraki
    Maltepe, Esra
    Chormey, Dotse Selali
    Bakirdere, Sezgin
    ENVIRONMENTAL MONITORING AND ASSESSMENT, 2020, 192 (02)
  • [30] Determination of fenazaquin in water and tomato matrices by GC-MS after a combined QuEChERS and switchable solvent liquid phase microextraction
    Nouha Bakaraki Turan
    Esra Maltepe
    Dotse Selali Chormey
    Sezgin Bakırdere
    Environmental Monitoring and Assessment, 2020, 192
12345