Combined cation exchange-liquid-liquid extraction method for GC-MS determination of 4-nonylphenol content in water

被引：0
|
作者：
Cruceru, Ioana [1 ]
Badea, Irinel Adriana [1 ]
Vladescu, Luminita [1 ]
机构：
[1] Univ Bucharest, Fac Chem, Dept Analyt Chem, Bucharest 030018, Romania
来源：
REVISTA DE CHIMIE | 2007年 / 58卷 / 12期
关键词：
4-nonylphenol; cation exchange-liquid-liquid extraction procedure; GC-MS;
D O I：
暂无
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
An efficient and highly selective combined cation exchange-liquid-liquid extraction method coupled with GC-MS determination is proposed for the separation and concentration of 4-nonylphenol from various water matrices. The method has good precision expressed as repeatability: mean value 97.28% with a RSD value of 4.20%. Recovery of alkylphenols from spiked samples varies from 92 to 101% and the values obtained are higher than with other methods currently in use. The method was successfully applied for the determination of 4-nonylphenol from various water matrices.
引用
收藏
页码：1305 / 1309
页数：5
相关论文
共 50 条
  • [1] Recovery of 4-nonylphenol and 4-nonylphenol ethoxylates from river sediments by pressurised liquid extraction
    Valsecchi, S
    Polesello, S
    Cavalli, S
    JOURNAL OF CHROMATOGRAPHY A, 2001, 925 (1-2) : 297 - 301
  • [2] Determination of Tramadol by Dispersive Liquid-Liquid Microextraction Combined with GC-MS
    Habibollahi, Saeed
    Tavakkoli, Nahid
    Nasirian, Vahid
    Khani, Hossein
    JOURNAL OF CHROMATOGRAPHIC SCIENCE, 2015, 53 (05) : 655 - 661
  • [3] METHOD COMPARISON FOR HERBICIDE DETERMINATION IN WATER - GC-MS VERSUS HPLC AND LIQUID LIQUID VERSUS SOLID-PHASE EXTRACTION
    STELLUTO, S
    MARCOMINI, A
    DICORCIA, A
    MARCHETTI, M
    CAPRI, S
    LIBERATORI, A
    ANNALI DI CHIMICA, 1990, 80 (7-8) : 369 - 377
  • [4] Determination of Bisphenol A and 4-Nonylphenol in Water Using Ionic Liquid Dispersive Liquid Phase Microextraction
    Sun, Aide
    Xu, Qingcai
    Yu, Xingxiu
    POLISH JOURNAL OF ENVIRONMENTAL STUDIES, 2013, 22 (03): : 899 - 907
  • [5] A Novel Liquid-Liquid Extraction for the Determination of Sertraline in Tap Water and Waste Water at Trace Levels by GC-MS
    Kocoglu, Elif Seda
    Bakirdere, Sezgin
    Keyf, Seyfullah
    BULLETIN OF ENVIRONMENTAL CONTAMINATION AND TOXICOLOGY, 2017, 99 (03) : 354 - 359
  • [6] Comparison of SPME to liquid-liquid extraction for the GC-MS determination of triclosan in water contaminated with OWC's
    Geary, Robert E.
    Waratuke, Stephen
    ABSTRACTS OF PAPERS OF THE AMERICAN CHEMICAL SOCIETY, 2013, 245
  • [7] A Novel Liquid-Liquid Extraction for the Determination of Nicotine in Tap Water, Wastewater, and Saliva at Trace Levels by GC-MS
    Dobrowska, Joanna Sonia
    Erarpat, Sezin
    Chormey, Dotse Selali
    Pyrzynska, Krystyna
    Bakirdere, Sezgin
    JOURNAL OF AOAC INTERNATIONAL, 2016, 99 (03) : 806 - 812
  • [8] Determination of endosulfan and some pyrethroids in waters by micro liquid-liquid extraction and GC-MS
    A. Fernández-Gutiérrez
    J. L. Martínez-Vidal
    F. J. Arrebola-Liébanas
    A. Gonzalez-Casado
    J. L. Vílchez
    Fresenius' Journal of Analytical Chemistry, 1998, 360 : 568 - 572
  • [9] Determination of endosulfan and some pyrethroids in waters by micro liquid-liquid extraction and GC-MS
    Fernandez-Gutierrez, A
    Martinez-Vidal, JL
    Arrebola-Liebanas, FJ
    Gonzalez-Casado, A
    Vilchez, JK
    FRESENIUS JOURNAL OF ANALYTICAL CHEMISTRY, 1998, 360 (05): : 568 - 572
  • [10] Equilibrium study on the reactive liquid-liquid extraction of 4-cyanopyridine with 4-nonylphenol
    Bokhove, J.
    Schuur, B.
    de Haan, A. B.
    CHEMICAL ENGINEERING SCIENCE, 2012, 82 : 215 - 222
12345