Influence of milling time on the structural, microstructural and magnetic properties of mechanically alloyed Ni58Fe12Zr10Hf10B10 nanostructured/amorphous powders

被引:16
|
作者
Besmel, R. [1 ]
Ghaffari, M. [2 ]
Shokrollahi, H. [3 ]
Chitsazan, B. [1 ]
Karimi, L. [1 ]
机构
[1] Islamic Azad Univ, Ahvaz Branch, Dept Mat Sci & Engn, Ahvaz, Iran
[2] Nanyang Technol Univ, Sch Elect & Elect Engn, Sensor & Actuator Lab 2, Singapore 639798, Singapore
[3] Shiraz Univ Technol, Electroceram Grp, Dept Mat Sci & Engn, Shiraz 71555313, Iran
关键词
Mechanical alloying; X-ray diffraction; Magnetic measurements; Amorphous materials; NI; NB; CO;
D O I
10.1016/j.jmmm.2011.05.025
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
This paper investigates structural, microstructural and magnetic properties of amorphous/nanocrystalline Ni58Fe12Zr10Hf10B10 powders prepared by high energy milling. Ball milling of Ni, Fe, Zr, Hf and B leads to alloying of the element powders at 120 h. The results show that at 190 h the amorphous content is at the highest level and the grain size is about 2 nm. The magnetic measurements reveal that the coercivity and the saturation magnetization reach about 20 Oe and 30 emu/g at 190 h and become approximately 5 Oe and 40 emu/g after a suitable heat treatment, respectively. (C) 2011 Elsevier B.V. All rights reserved.
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页码:2727 / 2733
页数:7
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