Synthesis and Characterization of Mesoporous Silicon Spheres from Solid Silica Spheres

被引:0
|
作者
Zhu, Jiang [1 ]
Meng, Changgong [1 ]
机构
[1] Dalian Univ Technol, Dept Chem, Dalian 116023, Peoples R China
来源
ADVANCED MATERIAL SCIENCE AND TECHNOLOGY, PTS 1 AND 2 | 2011年 / 675-677卷
关键词
porous silicon; mesoporous; sphere; magnesiothermal; polycrystal; REDUCTION; SI;
D O I
10.4028/www.scientific.net/MSF.675-677.1069
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
A well known method was used to convert the solid silica spheres to porous silicon spheres with high surface area, with the starting shape retained. The presented work demonstrated that the porous silicon spheres are composed of polycrystal morphology. Due to the quantum confinement effect, the photoluminescence emission centered at 621 nm. The results of N-2 adsorption and desorption analysis indicates the mesoporous silicon spheres possess a surface area around 88 m(2) g(-1) and single point micro-pore volume 0.173 cm(3) g(-1).
引用
收藏
页码:1069 / 1072
页数:4
相关论文
共 50 条
  • [11] Catalytic Characterization of Mesoporous Ti–Silica Hollow Spheres
    M. Baca
    W. J. Li
    P. Du
    G. Mul
    J. A. Moulijn
    M.-O. Coppens
    Catalysis Letters, 2006, 109 : 207 - 210
  • [12] Synthesis and Characterization of Hollow Mesoporous Silica Spheres and Studying the Load and Release of Dexamethasone
    Al Roaya, M. Amin
    Manteghi, F.
    Haghverdi, M.
    SILICON, 2019, 11 (03) : 1401 - 1411
  • [13] Synthesis and Characterization of Hollow Mesoporous Silica Spheres and Studying the Load and Release of Dexamethasone
    M. Amin Al Roaya
    F. Manteghi
    M. Haghverdi
    Silicon, 2019, 11 : 1401 - 1411
  • [14] Synthesis of hollow spheres with mesoporous silica nanoparticles shell
    Yang, Mu
    Wang, Ge
    Yang, Zhenzhong
    MATERIALS CHEMISTRY AND PHYSICS, 2008, 111 (01) : 5 - 8
  • [15] Synthesis of artificial opals with uniform mesoporous silica spheres
    Chen, CN
    Lin, HP
    Tsai, CP
    Tang, CY
    CHEMISTRY LETTERS, 2004, 33 (07) : 838 - 839
  • [16] Synthesis of ZnS nanoparticles into the pore of mesoporous silica spheres
    Li, Yaoxia
    Zhu, Yihua
    Li, Cuiyan
    Yang, Xiaoling
    Li, Chunzhong
    MATERIALS LETTERS, 2009, 63 (12) : 1068 - 1070
  • [17] Mesoporous Carbon Spheres: Synthesis, Characterization and Supercapacitance
    Chen, Jingxing
    Xia, Nannan
    Zhou, Tianxiang
    Tan, Sanxiang
    Jiang, Fengping
    Yuan, Dingsheng
    INTERNATIONAL JOURNAL OF ELECTROCHEMICAL SCIENCE, 2009, 4 (08): : 1063 - 1073
  • [18] Synthesis and Characterization of Mesoporous Titanium Dioxide Spheres
    Guli Mi-na
    Chen Yu-ning
    Li Xiao-tian
    CHEMICAL RESEARCH IN CHINESE UNIVERSITIES, 2011, 27 (03) : 350 - 353
  • [19] Synthesis and Characterization of Mesoporous Titanium Dioxide Spheres
    GULI Mi-na1
    2. Key Laboratory of Automobile Materials of Ministry of Education
    ChemicalResearchinChineseUniversities, 2011, 27 (03) : 350 - 353
  • [20] Synthesis of monodisperse silica spheres with solid core and mesoporous shell: Morphological control of mesopores
    Kim, Jung Ho
    Yoon, Suk Bon
    Kim, Jong-Yun
    Chae, Young Bae
    Yu, Jong-Sung
    COLLOIDS AND SURFACES A-PHYSICOCHEMICAL AND ENGINEERING ASPECTS, 2008, 313 : 77 - 81