Suspended CaSO4 center dot 2H(2)O was recrystd. to CaSO4 center dot 0.5H(2)O (I) in aq. soln. of H3PO4(24-28% by mass of P2O5, 4-8% by mass of SO42-) at 88-92 degrees C for 1-4 h to det. the optimum conditions. The I content in the solid phase increased up to above 90% (conversion degree near to 100%) with the increasing temp., and P2O5 and SO42- contents in the soln.
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Rudjer Boskovic Inst, Div Mat Chem, Lab Precipitat Proc, HR-10002 Zagreb, CroatiaRudjer Boskovic Inst, Div Mat Chem, Lab Precipitat Proc, HR-10002 Zagreb, Croatia
Kontrec, J
Kralj, D
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Rudjer Boskovic Inst, Div Mat Chem, Lab Precipitat Proc, HR-10002 Zagreb, CroatiaRudjer Boskovic Inst, Div Mat Chem, Lab Precipitat Proc, HR-10002 Zagreb, Croatia
Kralj, D
Brecevic, L
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Rudjer Boskovic Inst, Div Mat Chem, Lab Precipitat Proc, HR-10002 Zagreb, CroatiaRudjer Boskovic Inst, Div Mat Chem, Lab Precipitat Proc, HR-10002 Zagreb, Croatia
机构:
Hebei Univ, Affiliated Hosp, Dept Orthoped, Baoding 071000, Peoples R ChinaHebei Univ, Affiliated Hosp, Dept Orthoped, Baoding 071000, Peoples R China
Liu, Yong
Wang, Hui
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JiZhong Energy Fengfeng Grp Co LTD, Gen Hosp, Handan 056002, Peoples R ChinaHebei Univ, Affiliated Hosp, Dept Orthoped, Baoding 071000, Peoples R China
Wang, Hui
Li, Ning
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Third Hosp Shijiazhuang, Shijiazhuang 050011, Peoples R ChinaHebei Univ, Affiliated Hosp, Dept Orthoped, Baoding 071000, Peoples R China
Li, Ning
Zhou, Xiaozhe
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Hebei Univ, Affiliated Hosp, Dept Orthoped, Baoding 071000, Peoples R ChinaHebei Univ, Affiliated Hosp, Dept Orthoped, Baoding 071000, Peoples R China
Zhou, Xiaozhe
Gao, Wenshan
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Hebei Univ, Affiliated Hosp, Dept Orthoped, Baoding 071000, Peoples R ChinaHebei Univ, Affiliated Hosp, Dept Orthoped, Baoding 071000, Peoples R China
Gao, Wenshan
Jiao, Jianbao
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Hebei Univ, Affiliated Hosp, Dept Orthoped, Baoding 071000, Peoples R ChinaHebei Univ, Affiliated Hosp, Dept Orthoped, Baoding 071000, Peoples R China