starch;
synthesis;
superabsorbent;
water absorbency;
microwave heating;
D O I:
10.4028/www.scientific.net/AMR.239-242.1854
中图分类号:
TQ [化学工业];
学科分类号:
0817 ;
摘要:
The aqueous solution polymerization methods were carried out using microwave heating for the superabsorbent synthesis experiment. The differences between reaction temperatures and reaction times were compared respectively under the same conventional heating conditions. The results showed that microwave heating can generate better results: The maximum of distilled water absorbency is 711 times, and the maximum of 0.9% saline water absorbency is 86 times when the polymerization temperature is at 35 degrees C and the reaction time is 1.5 h. Water absorbency of the superabsorbent obtained using microwave heating is better than that of conventional heating. Analysis of FTIR and SEM showed that starch grafting with acrylic acid and acrylamide was successful, and a three-dimensional network structure was formed in superabsorbent. The causes of organic reactions accelerated using microwave heating were also discussed in this paper.
机构:
Yancheng Inst Technol, Coll Text & Clothing, Yancheng, Jiangsu, Peoples R ChinaYancheng Inst Technol, Coll Text & Clothing, Yancheng, Jiangsu, Peoples R China
Hu, Xiaosai
Wang, Chenyang
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机构:
Yancheng Inst Technol, Coll Text & Clothing, Yancheng, Jiangsu, Peoples R ChinaYancheng Inst Technol, Coll Text & Clothing, Yancheng, Jiangsu, Peoples R China
Wang, Chenyang
Yu, Haiyang
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机构:
Yancheng Inst Technol, Coll Text & Clothing, Yancheng, Jiangsu, Peoples R ChinaYancheng Inst Technol, Coll Text & Clothing, Yancheng, Jiangsu, Peoples R China
机构:
S China Univ Technol, Coll Chem & Chem Technol, Guangzhou 510641, Guangdong, Peoples R ChinaS China Univ Technol, Coll Chem & Chem Technol, Guangzhou 510641, Guangdong, Peoples R China
Ge, Huacai
Wang, Senkang
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机构:
S China Univ Technol, Coll Chem & Chem Technol, Guangzhou 510641, Guangdong, Peoples R ChinaS China Univ Technol, Coll Chem & Chem Technol, Guangzhou 510641, Guangdong, Peoples R China
机构:
CENAM, Queretaro 76246, MexicoUniv Autonoma Queretaro, Div Invest & Postgrad, Fac Ingn, Queretaro 76010, Qro, Mexico
Cabrera, J. L.
Velazquez-Castillo, R.
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机构:
Univ Autonoma Queretaro, Div Invest & Postgrad, Fac Ingn, Queretaro 76010, Qro, MexicoUniv Autonoma Queretaro, Div Invest & Postgrad, Fac Ingn, Queretaro 76010, Qro, Mexico
Velazquez-Castillo, R.
Rivera-Munoz, E. M.
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机构:
Univ Nacl Autonoma Mexico, Ctr Fis Aplicada & Tecnol Avanzada, Queretaro 76000, Qro, MexicoUniv Autonoma Queretaro, Div Invest & Postgrad, Fac Ingn, Queretaro 76010, Qro, Mexico