Effect of the milling conditions on the formation of nanostructured Fe-Co powders

被引:27
|
作者
Alleg, Safia [1 ]
Bentayeb, Fatima Zohra [1 ]
Bensalem, Rachid [1 ]
Djebbari, Chafia [1 ]
Bessais, Lotfi [2 ]
Greneche, Jean Marc [3 ]
机构
[1] Univ Annaba, Fac Sci, Dept Phys, Lab Magnetisme & Spect Solides, Annaba 23000, Algeria
[2] CNRS, Lab Chim Met Terres Rares, Grp Labs Thiais, F-94320 Thiais, France
[3] Univ Maine, CNRS, UMR 6087, Lab Phys Etat Condense, F-72085 Le Mans, France
关键词
D O I
10.1002/pssa.200824040
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
Nanostructured Fe-12Co (wt%) powders were prepared by mechanical alloying in a planetary ball mill. The milling process was carried out at different milling conditions. The obtained powders were characterized by X-ray diffraction, Fe-57 Mossbauer spectrometry and magnetic measurements. The low and high speed ball-milling conditions lead to the formation of a single and two-bcc Fe(Co) structure, respectively, having different crystallite sizes, microstrains hyper-fine parameters and magnetic properties. The average hyper-fine magnetic field values: < B >(1) = 34.8 T and < B >(2) = 28.2 T of the two-bcc Fe(Co) structure could be attributed to the nanocrystalline grains and to the grain boundaries, respectively. (c) 2008 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.
引用
收藏
页码:1641 / 1646
页数:6
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