Influence of Polyols on the Formation of Iron Oxide Nanoparticles in Solvothermal System

被引：6
|
作者：
Jiao, Shihui [1 ]
Xu, Man [1 ]
Zhang, Yingwei [1 ]
Pang, Guangsheng [1 ]
Feng, Shouhua [1 ]
机构：
[1] Jilin Univ, Coll Chem, State Key Lab Inorgan Synth & Preparat Chem, Changchun 130012, Peoples R China
来源：
JOURNAL OF NANOSCIENCE AND NANOTECHNOLOGY | 2010年 / 10卷 / 12期
基金：
中国国家自然科学基金;
关键词：
Nanoparticles; Solvothermal; Iron Oxide; Polyol; MAGNETITE HOLLOW SPHERES; GAMMA-FE2O3; PARTICLES; FE3O4; NANOPARTICLES; NANOMETER-SIZE; MONODISPERSE; NANOCRYSTALS; PROPERTY; ROUTE;
D O I：
10.1166/jnn.2010.3015
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
We reported a simple solvothermal route in phase-controllable synthesis of iron oxide nanoparticles by using polyols as solvent. Magnetite and hematite are selectively synthesized while Fe(NO3)(3)center dot 9H(2)O is used as single iron source and without any additives. While ethylene glycol, 1,2-propanediol, 1,3-butanediol, or glycerol is used as solvents, magnetite nanoparticles are obtained, and the average particle sizes vary from 10 to 40 nm. While 1,4-butanediol or 1,5-pentanediol is used as solvents, hematite nanoparticles are obtained. Our results suggest that the polyols with neighboring hydroxyl groups is favorable for the formation of magnetite nanoparticles.
引用
收藏
页码：8405 / 8407
页数：3
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