Determination of Phenolic Disinfectants in Consumer Products by Capillary Electrophoresis with Amperometric Detection

被引:5
|
作者
Jiang, Lianmei [1 ]
Wang, Jinyan [1 ]
He, Yan [1 ]
Ye, Jiannong [1 ]
Chu, Qingcui [1 ]
机构
[1] E China Normal Univ Chem, Shanghai 200062, Peoples R China
基金
中国国家自然科学基金;
关键词
TRICLOSAN; PROFILES;
D O I
10.1093/chromsci/48.7.584
中图分类号
Q5 [生物化学];
学科分类号
071010 ; 081704 ;
摘要
Numerous disinfection products are widely used in daily life to kill pathogenic microorganisms. However, most disinfectants are organic compounds that might be hazardous to the environment and humans when used excessively. Phenolic disinfectants in disinfection products are investigated using a high-performance capillary electrophoresis-amperometric detection method. Under the optimum conditions, five commonly used disinfectants can be well-separated within 19 min at the separation voltage of 18 kV in a 80 mmol/L borax running buffer (pH 9.2), and adequate extraction was obtained with ethanol for the determination of the five compounds. Satisfactory recovery (93.5-106.0%), intra-day repeatability of the peak current (< 2.9%), and detection limits (1.6 × 10-7 - 3.8 × 10-8 g/mL) for the method are achieved. This proposed procedure is successfully used to analyze different samples of disinfection products.
引用
收藏
页码:584 / 588
页数:5
相关论文
共 50 条
  • [41] Determination of aromatic amines in water samples by capillary electrophoresis with amperometric detection
    Sun, Yan
    Liang, Liyun
    Zhao, Xiaoyin
    Yu, Lin
    Zhang, Jie
    Shi, Guoyue
    Zhou, Tianshu
    WATER RESEARCH, 2009, 43 (01) : 41 - 46
  • [42] Fast determination of aldehyde preservatives by miniaturized capillary electrophoresis with amperometric detection
    Li, Ying
    Chen, Fang
    Ge, Jinyuan
    Tong, Fanghong
    Deng, Zhaoyue
    Shen, Fengwu
    Gu, Qianxia
    Ye, Jiannong
    Chu, Qingcui
    ELECTROPHORESIS, 2014, 35 (2-3) : 419 - 424
  • [43] Determination of dissociation constants of anthrocycline by capillary zone electrophoresis with amperometric detection
    Hu, Q
    Hu, G
    Zhou, TS
    Fang, YZ
    JOURNAL OF PHARMACEUTICAL AND BIOMEDICAL ANALYSIS, 2003, 31 (04) : 679 - 684
  • [44] Determination of ionization constants of saccharides by capillary zone electrophoresis with amperometric detection
    X. M. Fang
    F. Y. Gong
    J. N. Ye
    Y. Z. Fang
    Chromatographia, 1997, 46 : 137 - 140
  • [45] Determination of chlorite in drinking water using capillary electrophoresis with amperometric detection
    Wallenborg, SR
    Dorholt, SM
    Faibushevich, A
    Lunte, CE
    ELECTROANALYSIS, 1999, 11 (05) : 362 - 366
  • [46] Separation and Determination of β-Blockers Doping in Urine by Capillary Electrophoresis Amperometric Detection
    Song Zi-Wang
    Tong Ping
    Zheng Li-Hui
    Zhang Lan
    CHINESE JOURNAL OF ANALYTICAL CHEMISTRY, 2008, 36 (12) : 1624 - 1628
  • [47] Analysis of alkyl polyglucosides in industrial products by capillary electrophoresis with pulsed amperometric detection
    Hübner, J
    Nguyen, A
    Turcu, F
    Melchior, D
    Kling, HW
    Gäb, S
    Schmitz, OJ
    ANALYTICAL AND BIOANALYTICAL CHEMISTRY, 2006, 384 (01) : 259 - 264
  • [48] Analysis of alkyl polyglucosides in industrial products by capillary electrophoresis with pulsed amperometric detection
    Jane Hübner
    Anh Nguyen
    Florin Turcu
    David Melchior
    Hans-Willi Kling
    Siegmar Gäb
    Oliver J. Schmitz
    Analytical and Bioanalytical Chemistry, 2006, 384 : 259 - 264
  • [49] Microchip electrophoresis with amperometric detection for a novel determination of phenolic compounds in olive oil
    del Pilar Godoy-Caballero, Maria
    Isabel Acedo-Valenzuela, Maria
    Galeano-Diaz, Teresa
    Costa-Garcia, Agustin
    Teresa Fernandez-Abedul, Maria
    ANALYST, 2012, 137 (21) : 5153 - 5160
  • [50] DETERMINATION OF PHENOLIC DISINFECTANTS BY CAPILLARY GAS-CHROMATOGRAPHY
    NOLTE, J
    MAYER, H
    PASCHOLD, B
    FRESENIUS ZEITSCHRIFT FUR ANALYTISCHE CHEMIE, 1986, 325 (01): : 20 - 23