Analysis of C2-C4 peroxyacyl nitrates and C1-C5 alkyl nitrates with a non-polar capillary column

被引：6

作者：

Glavas, S ^{[1
]}

机构：

[1] Univ Patras, Dept Chem, EL-26500 Patras, Hellas, Greece

来源：

JOURNAL OF CHROMATOGRAPHY A | 2001年 / 915卷 / 1-2期

关键词：

air analysis; peroxyacyl nitrates; alkyl nitrates; tetrachloroethylene; carbon tetrachloride; chloroform; volatile organic compounds;

D O I：

10.1016/S0021-9673(01)00618-5

中图分类号：

Q5 [生物化学];

学科分类号：

071010 ; 081704 ;

摘要：

Analysis of peroxyacetyl nitrate (PAN), peroxypropionyl nitrate, peroxy-rt-butyryl nitrate, and peroxyisobutyryl nitrate (PiBN) with a non-polar capillary column indicated PAN not to coelute with PiBN. Isopropyl nitrate coeluted with PAN, n-butyl nitrate with PiBN and ethyl nitrate with chloroform, at oven temperature 30 degreesC. In addition methyl nitrate, n-propyl nitrate, 2-butyl nitrate, 2-methyl-2-butyl nitrate, 3-pentyl nitrate and 2-pentyl nitrate were studied. Their response factors in the electron-capture detector were also determined. Tetrachloroethylene, carbon tetrachloride and chloroform whose vapors occur in the atmosphere were also examined. (C) 2001 Elsevier Science B.V. All rights reserved.

引用

页码：271 / 274

页数：4

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