Synthesis of Task Specific and Reusable Protic Ionic Liquids for One-Pot Multicomponent Syntheses

被引：1

作者：

Sardar, Sabahat ^{[1
]}

Wilfred, Cecilia Devi ^{[1
]}

Marc, Leveque Jean ^{[1
]}

机构：

[1] Univ Teknol PETRONAS, Dept Fundamental & Appl Sci, Tronoh, Perak, Malaysia

来源：

PROCEEDING OF THE 4TH INTERNATIONAL CONFERENCE OF FUNDAMENTAL AND APPLIED SCIENCES 2016 (ICFAS2016) | 2016年 / 1787卷

关键词：

MANNICH REACTION; AROMATIC-ALDEHYDES;

D O I：

10.1063/1.4968075

中图分类号：

O59 [应用物理学];

学科分类号：

摘要：

Protic ionic liquids (ILs) synthesized from 1-methylimidazole with 1,3-propane sultone and 1,4-butane sultone catalyzed Mannich reaction at 25 degrees C to afford Mannich bases in high yield (76%) and less time duration (20 min). Ionic liquids have been used as dual reagent i.e., as catalyst as well as solvent. Simple extraction by water separated ionic liquid from reaction mixture with 4 times recycling without any significant loss in activity.

引用

页数：7

共 50 条

[21] One-pot Synthesis of Lewis Acidic Ionic Liquids for Friedel-Crafts Alkylation
Ling HE
ChineseChemicalLetters, 2006, (03) : 321 - 324
[22] Three-component coupling reactions in ionic liquids: One-pot synthesis of isoxazolidines
Yadav, J. S.
Reddy, B. V. S.
Sreedhar, P.
Murthy, Ch. V. S. R.
Mahesh, G.
Kondaji, G.
Nagaiah, K.
JOURNAL OF MOLECULAR CATALYSIS A-CHEMICAL, 2007, 270 (1-2) : 160 - 163
[23] Novel one-pot synthesis of quaternary ammonium halides: new route to ionic liquids
Ropponen, J
Lahtinen, M
Busi, S
Nissinen, M
Kolehmainen, E
Rissanen, K
NEW JOURNAL OF CHEMISTRY, 2004, 28 (12) : 1426 - 1430
[24] One-pot synthesis of Lewis acidic ionic liquids for Friedel-Crafts alkylation
He, L
Tao, GH
Liu, WS
Xiong, W
Wang, T
Kou, Y
CHINESE CHEMICAL LETTERS, 2006, 17 (03) : 321 - 324
[25] Three-component one-pot synthesis of α-hydroxylamino phosphonates using ionic liquids
Yadav, JS
Reddy, BVS
Sreedhar, P
ADVANCED SYNTHESIS & CATALYSIS, 2003, 345 (05) : 564 - 567
[26] Straightforward one-pot synthesis of benzofuroxans from o-halonitrobenzenes in ionic liquids
Sheremetev, Aleksei B.
Aleksandrov, Nataliya S.
Ignat'ev, Nikolai V.
Schulte, Michael
MENDELEEV COMMUNICATIONS, 2012, 22 (02) : 95 - 97
[27] One Pot Multicomponent Biginelli Reaction Employing Ionic Liquids as an Organocatalyst
Shaikh, Tanveer M.
Nagarajan, Sankaranarayanan
Kandasamy, Elango
CURRENT ORGANOCATALYSIS, 2020, 7 (02) : 96 - 107
[28] One-Pot Three-Component Synthesis of Spirooxindoles Catalyzed by Basic Ionic Liquids
Guo, Hongyun
Tian, Jinjin
CHINESE JOURNAL OF ORGANIC CHEMISTRY, 2011, 31 (05) : 752 - 756
[29] One-pot multicomponent synthesis of some novel acridines
Nadaraj, V.
Kalaivani, S.
Selvi, S. Thamarai
INDIAN JOURNAL OF CHEMISTRY SECTION B-ORGANIC CHEMISTRY INCLUDING MEDICINAL CHEMISTRY, 2007, 46 (10): : 1703 - 1706
[30] A straightforward one-pot multicomponent synthesis of polysubstituted pyrroles
Lin, Xufeng
Mao, Zhenjun
Dai, Xixiang
Lu, Ping
Wang, Yanguang
CHEMICAL COMMUNICATIONS, 2011, 47 (23) : 6620 - 6622

← 1 2 3 4 5 →