Fe(HSO4)3 as an efficient catalyst for the preparation of 3,4-dihydropyrimidin-2(1H)-ones in solution and under solvent-free conditions

被引：44

作者：

Shirini, F. ^{[1
]}

Zolfigol, M. A. ^{[2
]}

Abri, A. -R. ^{[1
]}

机构：

[1] Univ Guilan, Coll Sci, Dept Chem, Rasht 41335, Iran

[2] Bu Ali Sina Univ, Fac Chem, Hamaden 6517838683, Iran

来源：

JOURNAL OF THE IRANIAN CHEMICAL SOCIETY | 2008年 / 5卷 / 01期

关键词：

3,4-dihydropyrimidin-2(1H)-ones; solvent-free conditions; Biginelli reaction; three-component condensation; Fe(HSO4)(3);

D O I：

10.1007/BF03245821

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

A one-pot three-component condensation of aromatic aldehydes, beta-ketoesters and urea or thiourea, efficiently promoted in the presence of Fe(HSO4)(3) in solution and under solvent-free conditions, produced 3,4-dihydropyrimidin-2(1H)-ones. The method offers several advantages including simple, easy and clean work-up procedure, relatively short reaction times and good to high yields of the products.

引用

页码：96 / 99

页数：4

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