Synthesis of crown analogs derived from bisnaphthol

被引：0
|
作者：
Kumar, S [1 ]
Mashraqui, SH [1 ]
机构：
[1] Univ Bombay, Dept Chem, Mumbai 400098, India
来源：
INDIAN JOURNAL OF CHEMISTRY SECTION B-ORGANIC CHEMISTRY INCLUDING MEDICINAL CHEMISTRY | 1998年 / 37卷 / 04期
关键词：
D O I：
暂无
中图分类号：
O62 [有机化学];
学科分类号：
070303 ; 081704 ;
摘要：
Bisnaphthol 1, a readily accessible bifunctional phenol, has been cyclocondensed with tosylates 2, 3 and 4 under KOH/THF condition to provide 1:1 dinaphthano crowns 5, 6 and 7, respectively. The later is detosylated with LiAlH4 to provide 8. Macrocyclization of 1 with m-xylylene dibromide 9 and p-xylylene dibromide 10 affords 3:3 condensed macrocycles 11 and 12, respectively. The structures are supported by elemental analysis, mass and NMR spectral data.
引用
收藏
页码：348 / 351
页数：4
相关论文
共 50 条
  • [21] SULFONAL ANALOGS DERIVED FROM TETRAHYDROTHIAPYRAN
    BARKENBUS, C
    MIDKIFF, VC
    JOURNAL OF ORGANIC CHEMISTRY, 1951, 16 (07): : 1047 - 1049
  • [22] NITROGEN ANALOGS OF CROWN ETHERS
    RICHMAN, JE
    ATKINS, TJ
    JOURNAL OF THE AMERICAN CHEMICAL SOCIETY, 1974, 96 (07) : 2268 - 2270
  • [23] Si analogs of crown ethers
    不详
    CHEMICAL & ENGINEERING NEWS, 2006, 84 (15) : 54 - 54
  • [24] Acyclic nucleotide analogs derived from 8-azapurines: Synthesis and antiviral activity
    Holy, A
    Dvorakova, H
    Jindrich, J
    Masojidkova, M
    Budesinsky, M
    Balzarini, J
    Andrei, G
    DeClercq, E
    JOURNAL OF MEDICINAL CHEMISTRY, 1996, 39 (20) : 4073 - 4088
  • [25] Synthesis and some biological properties of sulfamates derived from 8α-analogs of steroidal estrogens
    Morozkina, S. N.
    Gluzdikov, I. A.
    Drozdov, A. S.
    Selivanov, S. I.
    Kovalev, R. A.
    Filatov, M. V.
    Shavva, A. G.
    RUSSIAN JOURNAL OF ORGANIC CHEMISTRY, 2015, 51 (03) : 411 - 416
  • [26] Synthesis and antitubercular activity of a series of hydrazone and nitrovinyl analogs derived from heterocyclic aldehydes
    Sonar, Vijayakumar N.
    Crooks, Peter A.
    JOURNAL OF ENZYME INHIBITION AND MEDICINAL CHEMISTRY, 2009, 24 (01) : 117 - 124
  • [27] Design and synthesis of new donepezil analogs derived from arylpiperazine scaffold as acetylcholinesterase inhibitors
    Sahin, Zafer
    Biltekin, Sevde Nur
    Buelbuel, Emre Fatih
    Yurttas, Leyla
    Berk, Barkin
    Demirayak, Seref
    PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS, 2020, 196 (03) : 283 - 293
  • [28] Synthesis and some biological properties of sulfamates derived from 8α-analogs of steroidal estrogens
    S. N. Morozkina
    I. A. Gluzdikov
    A. S. Drozdov
    S. I. Selivanov
    R. A. Kovalev
    M. V. Filatov
    A. G. Shavva
    Russian Journal of Organic Chemistry, 2015, 51 : 411 - 416
  • [29] Synthesis of 4-hydroxycyclopentenone-derived analogs and libraries
    Singh, Gurpreet
    Meyer, Angelica
    Aube, Jeffrey
    ABSTRACTS OF PAPERS OF THE AMERICAN CHEMICAL SOCIETY, 2014, 248
  • [30] SYNTHESIS OF BENZO-15-CROWN-5 POLYETHERS, ANTICOCCIDIAL IONOPHORE ANALOGS
    BROWN, GR
    FOUBISTER, AJ
    JOURNAL OF MEDICINAL CHEMISTRY, 1979, 22 (08) : 997 - 999
12345