Assembly of two Cu-based coordination polymers from 2-(pyridine-3-yl)-1H-4,5-imidazoledicarboxylate ligand

被引：9
|
作者：
Dai, Cong [1 ]
Zhou, Xiaoying [1 ]
Jing, Xuemin [2 ]
Li, Guanghua [1 ]
Huo, Qisheng [1 ]
Liu, Yunling [1 ]
机构：
[1] Jilin Univ, Coll Chem, State Key Lab Inorgan Synth & Preparat Chem, Changchun 130012, Peoples R China
[2] Langfang Teachers Coll, Fac Chem & Mat Sci, Langfang 065000, Peoples R China
来源：
INORGANIC CHEMISTRY COMMUNICATIONS | 2015年 / 52卷
关键词：
Coordination polymer; 2-(Pyridine-3-yl)-1H-4,5-imidazoledicarboxylic acid; Three dimensional framework; Supramolecular structure; METAL-ORGANIC FRAMEWORKS; CONSTRUCTION; ACID; SQUARES; DESIGN; ZMOFS;
D O I：
10.1016/j.inoche.2015.01.010
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
Two novel Cu-based coordination polymers [Cu-5(HPyImDC)(4)]center dot(NH4)(3) (1) and [Cu-3(H2O)(2)(HPyImDC)(2) (C3N2H10)] (2) containing the 2-(pyridine-3-yl)-1H-4,5-imidazoledicarboxylate (H(3)PyImDC) ligand have been solvothermally synthesized. Single crystal X-ray diffraction analysis reveals that compound 1 exhibits a three dimensional framework with 1D rhombic channels, which can be simplified into a novel (3,4)-connected network with Schlafli symbol of (6(2).14(4))(6(2).8)(4). Compound 2 is one dimensional chain which packed with each other via n it and hydrogen-bonding interactions to construct a three dimensional supramolecular structure. As the first example related to Cu (I) and Cu (I, II) coordination polymers based on H(3)PyImDC ligands, compounds 1 and 2 are further studied by elemental analyses, IR spectroscopy and thermogravimetric analyses. (C) 2015 Elsevier B.V. All rights reserved.
引用
收藏
页码：69 / 72
页数：4
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