3-Chloro-N′-(3-ethoxy-2-hydroxybenzylidene)benzohydrazide monohydrate

被引：1
|
作者：
Li, Tian-Yi [1 ]
Zeng, Peng-Tao [1 ]
机构：
[1] Changchun Univ Technol, Sch Chem Engn, Changchun 130012, Peoples R China
来源：
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2011年 / 67卷
关键词：
CRYSTAL-STRUCTURE; COMPLEXES; HYDRAZONE; LIGAND;
D O I：
10.1107/S160053681100122X
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
In the title compound, C16H15ClN2O3 center dot H2O, the water molecule is linked to the Schiff base molecule via an O-H center dot center dot center dot O hydrogen bond. In the Schiff base molecule, an intramolecular O-H center dot center dot center dot N hydrogen bond occurs and the dihedral angle between the two benzene rings is 20.5 (5)degrees. In the crystal, the Schiff base and water molecules are linked by intermolecular N-H center dot center dot center dot O and O-H center dot center dot center dot O hydrogen bonds, forming layers in the ab plane.
引用
收藏
页码：O377 / U730
页数：9
相关论文
共 50 条
  • [21] (2E)-2-(3-Ethoxy-2-hydroxybenzylidene)-hydrazinecarboxamide
    Aravindakshan, A. Ambili
    Sithambaresan, M.
    Kurup, M. R. Prathapachandra
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2013, 69 : O586 - +
  • [22] Syntheses and Crystal Structures of 3-Chloro-N'-(3,5-dichloro-2-hydroxybenzylidene)-benzohydrazide and Its Oxovanadium(V) Complex with Antimicrobial Activity
    高栓平
    Chinese Journal of Structural Chemistry, 2012, (03) : 377 - 384
  • [23] 3-Chloro-N′-(4-hydroxy-3-nitrobenzylidene)benzohydrazide methanol disolvate
    Zhang, Zhen
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : O1630 - U191
  • [24] 3-Chloro-N′-(2-hydroxybenzylidene)benzohydrazide: An LSD1-Selective Inhibitor and Iron-Chelating Agent for Anticancer Therapy
    Sarno, Federica
    Papulino, Chiara
    Franci, Gianluigi
    Andersen, Jeanette H.
    Cautain, Bastien
    Melardo, Colombina
    Altucci, Lucia
    Nebbioso, Angela
    FRONTIERS IN PHARMACOLOGY, 2018, 9
  • [25] 2-Ethoxy-6-({2-[(3-ethoxy-2-hydroxybenzylidene)amino]benzyl}iminomethyl) phenol
    Ambili, K. U.
    Sreejith, S. S.
    Jacob, Jinsa Mary
    Sithambaresan, M.
    Kurup, M. R. Prathapachandra
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : 02482 - +
  • [26] N,N′-Bis(3-ethoxy-2-hydroxybenzylidene)-phenylene-1,3-diamine Methanol Solvate
    Osypiuk, Dariusz
    Bartyzel, Agata
    Cristovao, Beata
    MOLBANK, 2023, 2023 (03)
  • [27] Synthesis and crystal structures of N′-(3-ethoxy-2-hydroxybenzylidene)-3-methylbenzohydrazide and its dioxomolybdenum(VI) complex
    Gao, Shuan-Ping
    JOURNAL OF COORDINATION CHEMISTRY, 2011, 64 (16) : 2869 - 2877
  • [28] Synthesis, Structures, and Antibacterial Activities of 3-Methoxy-N′-(3-bromo-5-chloro-2-hydroxybenzylidene)benzohydrazide Dimethanol Solvates and 3-Hydroxy-N′-(3-bromo-5-chloro-2-hydroxybenzylidene)benzohydrazide Methanol Solvate
    Zhu, Q. -Y.
    Wei, Y. -J.
    Wang, F. -W.
    POLISH JOURNAL OF CHEMISTRY, 2009, 83 (07) : 1233 - 1240
  • [29] 2-chloro-N′-(3,5-dibromo-2-hydroxybenzylidene) benzohydrazide methanol solvate
    Tang, Chun-Bao
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2008, 64 : O1382 - U1268
  • [30] Redetermination of the crystal structure of N′-(3-ethoxy-2-hydroxybenzylidene)-4-fluorobenzohydrazide monohydrate, C16H17FN2O4
    Lo, Kong Mun
    Lee, See Mun
    Tiekink, Edward R. T.
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE-NEW CRYSTAL STRUCTURES, 2020, 235 (02): : 259 - 261
12345